3-Methoxy-5-nitrobenzamide

Base Information

Chemical Name:3-Methoxy-5-nitrobenzamide
CAS No.:292635-40-6
Molecular Formula:C8H8N2O4
Molecular Weight:196.163
Hs Code.:
DSSTox Substance ID:DTXSID40395260
Nikkaji Number:J169.164C
Mol file:292635-40-6.mol

Synonyms:3-methoxy-5-nitrobenzamide;292635-40-6;5-methoxy-3-nitrobenzamide;Oprea1_631309;SCHEMBL1719601;DTXSID40395260;WWUGAZZJZSTOBD-UHFFFAOYSA-N;STK365895;AKOS005442721;BS-22234

Suppliers and Price of 3-Methoxy-5-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Methoxy-5-nitrobenzamide

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:196.04840674
Heavy Atom Count:14
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1)[N+](=O)[O-])C(=O)N

Technology Process of 3-Methoxy-5-nitrobenzamide

There total 3 articles about 3-Methoxy-5-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 78238-13-8
3-methoxy-5-nitrobenzoic acid methyl ester

: 292635-40-6
3-methoxy-5-nitrobenzamide

Guidance literature:: With ammonium hydroxide; In methanol; at 20 ℃; for 120h;
DOI:10.1021/ol0612760

Reference yield:

: 85276-68-2
3-methoxy-5-nitrobenzoyl chloride

: 292635-40-6
3-methoxy-5-nitrobenzamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; at 0 - 10 ℃; Concentration;

Reference yield:

: 99-34-3
3,5-dinitrobenzoic acid

: 292635-40-6
3-methoxy-5-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 15 h / 20 - 80 °C

2: N,N-dimethyl-formamide; thionyl chloride / tetrahydrofuran / 1 h / Reflux

3: ammonium hydroxide / tetrahydrofuran / 0 - 10 °C

With ammonium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dimethyl sulfoxide;