(cyclohexylimino)(triphenyl)-lambda~5~-phosphane

Base Information

Chemical Name:(cyclohexylimino)(triphenyl)-lambda~5~-phosphane
CAS No.:66949-28-8
Molecular Formula:C24H26NP
Molecular Weight:359.451
Hs Code.:

Synonyms:

Suppliers and Price of (cyclohexylimino)(triphenyl)-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of (cyclohexylimino)(triphenyl)-lambda~5~-phosphane

Chemical Property:

Vapor Pressure:9.56E-10mmHg at 25°C
Boiling Point:502.9°Cat760mmHg
Flash Point:257.9°C
Density:1.08g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (cyclohexylimino)(triphenyl)-lambda~5~-phosphane

There total 4 articles about (cyclohexylimino)(triphenyl)-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₄H₂₆NP*ClH

: 66949-28-8
(cyclohexylimino)triphenylphosphorane

Guidance literature:: With polystyrene supported BEMP; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja409121s

Reference yield:

: 108-85-0
1-bromocyclohexane

: 66949-28-8
(cyclohexylimino)triphenylphosphorane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / dimethyl sulfoxide / 16 h / 60 °C

2.1: diethyl ether / 20 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: polystyrene supported BEMP / dichloromethane / 1 h / 20 °C / Inert atmosphere

With sodium azide; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja409121s

Reference yield:

: 19573-22-9
cyclohexyl azide

: 66949-28-8
(cyclohexylimino)triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 20 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: polystyrene supported BEMP / dichloromethane / 1 h / 20 °C / Inert atmosphere

With polystyrene supported BEMP; In diethyl ether; dichloromethane;
DOI:10.1021/ja409121s