4-(p-Chlorophenyl)-3-methyl-3-butenoic acid

Base Information

Chemical Name:4-(p-Chlorophenyl)-3-methyl-3-butenoic acid
CAS No.:91121-52-7
Molecular Formula:C₁₁H₁₁ClO₂
Molecular Weight:210.66
Hs Code.:
Nikkaji Number:J70.088F
Wikidata:Q76313757

Synonyms:BRN 2576946;4-(p-Chlorophenyl)-3-methyl-3-butenoic acid;3-BUTENOIC ACID, 4-(p-CHLOROPHENYL)-3-METHYL-;91121-52-7;AKOS022650312;LS-47112;4-(4-CHLOROPHENYL)-3-METHYL-3-BUTENOIC ACID

Suppliers and Price of 4-(p-Chlorophenyl)-3-methyl-3-butenoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-(p-Chlorophenyl)-3-methyl-3-butenoic acid

Chemical Property:

Vapor Pressure:7.66E-06mmHg at 25°C
Boiling Point:361°Cat760mmHg
Flash Point:172.1°C
Density:1.24g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:210.0447573
Heavy Atom Count:14
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC1=CC=C(C=C1)Cl)CC(=O)O
Isomeric SMILES:C/C(=C\C1=CC=C(C=C1)Cl)/CC(=O)O

Technology Process of 4-(p-Chlorophenyl)-3-methyl-3-butenoic acid

There total 3 articles about 4-(p-Chlorophenyl)-3-methyl-3-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5219-07-8
2-(4-chlorophenyl)-3-oxobutanenitrile

: 91121-52-7
4-(4-chlorophenyl)-3-methyl-3-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O, H₂SO₄

2: 1. CH₃ONa, 2. KOH / 1) methanol, dimethylformamide, 20 deg C, 4 h; 2) 8 h, 110 deg C; 3) reflux with 10percent KOH in mixture ethanol water 1:1

With potassium hydroxide; sulfuric acid; water; sodium methylate;
DOI:10.1135/cccc19840122

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 5586-88-9
1-(4-chlorophenyl)propan-2-one

: 91121-52-7
4-(4-chlorophenyl)-3-methyl-3-butenoic acid

: 91121-51-6
4-(4-chlorophenyl)-3-methyl-2-butenoic acid

Guidance literature:: With potassium hydroxide; sodium methylate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) methanol, dimethylformamide, 20 deg C, 4 h ; 2) 8 h, 110 deg C ; 3) reflux with 10percent KOH in mixture ethanol water 1:1;
DOI:10.1135/cccc19840122