8(2),8(2)-Difluoroprotoporphyrin dimethyl ester

Base Information

Chemical Name:8(2),8(2)-Difluoroprotoporphyrin dimethyl ester
CAS No.:123279-54-9
Molecular Formula:C₃₆H₃₆F₂N₄O₄
Molecular Weight:626.703
Hs Code.:
Mol file:123279-54-9.mol

Synonyms:21H,23H-Porphine-2,18-dipropanoic acid,7-(2,2-difluoroethenyl)-12-ethenyl-3,8,13,17-tetramethyl-,dimethyl ester;methyl 3-[7-(2,2-difluoroethenyl)-12-ethenyl-18-(3-methoxy-3-oxopropyl)-3,8,13,17-tetramethyl-22,23-dihydroporphyrin-2-yl]propanoate;8(2),8(2)-Difluoroprotoporphyrin dimethyl ester;8-Fppd;Dimethyl 7-(2,2-difluoroethenyl)-12-ethenyl-3,8,13,17-tetramethyl-21H,23H-porphine-2,18-dipropanoate;

Suppliers and Price of 8(2),8(2)-Difluoroprotoporphyrin dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8(2),8(2)-Difluoroprotoporphyrin dimethyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:1018.1°Cat760mmHg
Flash Point:569.5°C
PSA：108.90000
Density:1.245g/cm³
LogP:5.00750

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8(2),8(2)-Difluoroprotoporphyrin dimethyl ester

There total 5 articles about 8(2),8(2)-Difluoroprotoporphyrin dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1895-39-2
sodium chlorodifluoroacetate

: 13187-15-0
8-formyl-3-vinyldeuteroporphyrin IX dimethyl ester

: 123279-54-9
8²,8²-difluoroprotoporphyrin dimethyl ester

Guidance literature:: With triphenylphosphine; In various solvent(s); at 160 ℃;
DOI:10.1248/cpb.38.2175

Reference yield:

: 62921-27-1
3,3'-[7-(1,2-dihydroxy-ethyl)-3,8,13,17-tetramethyl-12-vinyl-21H,23H-porphine-2,18-diyl]-bis-propionic acid dimethyl ester

: 123279-54-9
8²,8²-difluoroprotoporphyrin dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / HIO₄, H₂O / dioxane / Ambient temperature

2: 42 percent / triphenylphosphine / various solvent(s) / 0.5 h / 160 °C

With water; periodic acid; triphenylphosphine; In 1,4-dioxane;
DOI:10.1016/S0022-1139(00)82758-X

Reference yield:

: 78422-39-6
3-[(5Z,10Z,14Z,19Z)-8-Hydroxy-7-[2-hydroxy-eth-(E)-ylidene]-18-(2-methoxycarbonyl-ethyl)-3,8,13,17-tetramethyl-12-vinyl-7,8,21,23-tetrahydro-porphin-2-yl]-propionic acid methyl ester

: 123279-54-9
8²,8²-difluoroprotoporphyrin dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / H⁺ / Ambient temperature

2: 82 percent / HIO₄, H₂O / dioxane / Ambient temperature

3: 42 percent / triphenylphosphine / various solvent(s) / 0.5 h / 160 °C

With water; hydrogen cation; periodic acid; triphenylphosphine; In 1,4-dioxane;
DOI:10.1016/S0022-1139(00)82758-X