Diethyl 4-nitroheptanedioate

Base Information

Chemical Name:Diethyl 4-nitroheptanedioate
CAS No.:2985-49-1
Molecular Formula:C11H19NO6
Molecular Weight:261.275
Hs Code.:
DSSTox Substance ID:DTXSID60398839
Nikkaji Number:J3.079.942I
Wikidata:Q82201051
Mol file:2985-49-1.mol

Synonyms:2985-49-1;Heptanedioic acid, 4-nitro-, diethyl ester;Diethyl 4-nitroheptanedioate;DTXSID60398839;4-Nitroheptanedioic acid diethyl ester;AKOS024340643

Suppliers and Price of Diethyl 4-nitroheptanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Diethyl 4-nitroheptanedioate

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:10
Exact Mass:261.12123733
Heavy Atom Count:18
Complexity:264

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CCC(CCC(=O)OCC)[N+](=O)[O-]

Technology Process of Diethyl 4-nitroheptanedioate

There total 4 articles about Diethyl 4-nitroheptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 75-52-5
nitromethane

: 140-88-5,9003-32-1
ethyl acrylate

: 2832-16-8
ethyl 4-nitrobutanoate

: 2985-49-1
diethyl 4-nitroheptanedioate

Guidance literature:: With potassium fluoride; In ethanol; at 20 ℃; for 2h;
DOI:10.1016/S0040-4039(99)01061-8

Reference yield: 36.0%

: 75-52-5
nitromethane

: 140-88-5,9003-32-1
ethyl acrylate

: 2832-16-8
ethyl 4-nitrobutanoate

: 2985-49-1
diethyl 4-nitroheptanedioate

: 86048-38-6
diethyl 4-nitro-4-<1-<2-(ethoxycarbonyl)ethyl>>heptanedioate

Guidance literature:: With N,N,N',N'-tetramethylguanidine; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200900009

Reference yield:

: 75-52-5
nitromethane

: 140-88-5,9003-32-1
ethyl acrylate

: 6317-49-3
4-oxopimelate

: 2985-49-1
diethyl 4-nitroheptanedioate

Guidance literature:: nitromethane; ethyl acrylate; With copper(l) cyanide; caesium carbonate; In dichloromethane; at 30 - 32 ℃; for 0.5h;

With water; In dichloromethane;
DOI:10.1016/j.tetlet.2012.04.071