2-(2-Azidophenyl)-1H-benzimidazole

Base Information

Chemical Name:2-(2-Azidophenyl)-1H-benzimidazole
CAS No.:29951-97-1
Molecular Formula:C13H9N5
Molecular Weight:235.248
Hs Code.:
DSSTox Substance ID:DTXSID70489141
Wikidata:Q82332245
Mol file:29951-97-1.mol

Synonyms:2-(2-Azidophenyl)-1H-benzimidazole;29951-97-1;DTXSID70489141

Suppliers and Price of 2-(2-Azidophenyl)-1H-benzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(2-Azidophenyl)-1H-benzimidazole

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:235.08579531
Heavy Atom Count:18
Complexity:338

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C2=NC3=CC=CC=C3N2)N=[N+]=[N-]

Technology Process of 2-(2-Azidophenyl)-1H-benzimidazole

There total 6 articles about 2-(2-Azidophenyl)-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 31162-13-7
2-azidobenzoic acid

: 95-54-5
1,2-diamino-benzene

: 29951-97-1
2-(2-azidophenyl)benzimidazole

Guidance literature:: With polyphosphoric ethyl ester; at 100 ℃; for 1h;

Reference yield: 72.0%

: 125701-38-4
N-(2-Amino-phenyl)-2-azido-benzamide

: 29951-97-1
2-(2-azidophenyl)benzimidazole

Guidance literature:: With sodium acetate; In acetic acid; for 1h; Heating;
DOI:10.1016/S0040-4020(01)81321-1

Reference yield:

: 31162-13-7
2-azidobenzoic acid

: 29951-97-1
2-(2-azidophenyl)benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / DCC / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT; 2 h,

2: 72 percent / AcONa / acetic acid / 1 h / Heating

With sodium acetate; dicyclohexyl-carbodiimide; In dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)81321-1