Technology Process of 11-Tetradecen-9-yn-1-ol, (11E)-
There total 9 articles about 11-Tetradecen-9-yn-1-ol, (11E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
for 24h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) lithium amide / 1.) liq. ammonia, 2 h, 2.) THF, -33 deg C, 6 h
2: 65 percent / triphenylphosphine, carbon tetrachloride / 6 h / Heating
3: 1.) CuI / 1.) ether, room temperature, 1 h, 2.) THF, 4 h, room temperature
4: 85 percent / PTS acid / methanol / 24 h / Ambient temperature
With
tetrachloromethane; copper(l) iodide; lithium amide; toluene-4-sulfonic acid; triphenylphosphine;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) lithium amide / 1.) liq. ammonia, 2 h, 2.) THF, -33 deg C, 6 h
2: 65 percent / triphenylphosphine, carbon tetrachloride / 6 h / Heating
3: 1.) CuI / 1.) ether, room temperature, 1 h, 2.) THF, 4 h, room temperature
4: 85 percent / PTS acid / methanol / 24 h / Ambient temperature
With
tetrachloromethane; copper(l) iodide; lithium amide; toluene-4-sulfonic acid; triphenylphosphine;
In
methanol;
