Carbamic acid, (3-phenylpropyl)-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, (3-phenylpropyl)-, phenylmethyl ester
CAS No.:302569-84-2
Molecular Formula:C17H19NO2
Molecular Weight:269.343
Hs Code.:
Mol file:302569-84-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (3-phenylpropyl)-, phenylmethyl ester

Chemical Property:

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Technology Process of Carbamic acid, (3-phenylpropyl)-, phenylmethyl ester

There total 13 articles about Carbamic acid, (3-phenylpropyl)-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 104-53-0
3-phenyl-propionaldehyde

: 621-84-1
O-benzyl carbamate

: 302569-84-2
N-benzyloxycarbonyloxy-3-phenylpropylamine

Guidance literature:: With triethylsilane; perrhenic acid anhydride; In dichloromethane; at 20 ℃; for 1.5h; chemoselective reaction;
DOI:10.1039/c2cc33185c

Reference yield: 71.0%

: 591-50-4
iodobenzene

: 39945-54-5
benzyl N-(3-bromopropyl)carbamate

: 92-52-4,1594-86-1
biphenyl

: 16644-57-8
N¹,N⁸-Dicarbobenzoxyhexanediamine

: 302569-84-2
N-benzyloxycarbonyloxy-3-phenylpropylamine

Guidance literature:: With pyridine; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; manganese; H₇I₂NiO_3.5; o-phenylenebis(diphenylphosphine); 4,4'-di-tert-butyl-2,2'-bipyridine; at 60 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ja9093956

Reference yield: 70.0%

: 108-86-1,52753-63-6
bromobenzene

: 39945-54-5
benzyl N-(3-bromopropyl)carbamate

: 92-52-4,1594-86-1
biphenyl

: 65095-17-2
N-(benzyloxycarbonyl)propylamine

: 16644-57-8
N¹,N⁸-Dicarbobenzoxyhexanediamine

: 302569-84-2
N-benzyloxycarbonyloxy-3-phenylpropylamine

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: With pyridine; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 4,4'-Dimethoxy-2,2'-bipyridin; NiI₂*3.5H₂O; sodium iodide; zinc; at 20 - 60 ℃; for 5h; chemoselective reaction;
DOI:10.1021/ja301769r