Benzenecarbothioic acid, 4-(1,1-dimethylethyl)-, S-2-pyridinyl ester

Base Information

Chemical Name:Benzenecarbothioic acid, 4-(1,1-dimethylethyl)-, S-2-pyridinyl ester
CAS No.:307930-88-7
Molecular Formula:C16H17NOS
Molecular Weight:271.37700
Hs Code.:
Mol file:307930-88-7.mol

Synonyms:4-tert-Butyl-thiobenzoic acid S-pyridin-2-yl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenecarbothioic acid, 4-(1,1-dimethylethyl)-, S-2-pyridinyl ester

Chemical Property:

PSA：55.26000
LogP:4.31160

Purity/Quality:

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Technology Process of Benzenecarbothioic acid, 4-(1,1-dimethylethyl)-, S-2-pyridinyl ester

There total 1 articles about Benzenecarbothioic acid, 4-(1,1-dimethylethyl)-, S-2-pyridinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2637-34-5,73018-10-7
2-Sulfanylpyridine

: 1710-98-1
p-tert-butyl benzoyl chloride

: 307930-88-7
S-2-pyridyl 4-tert-butylbenzothioate

Guidance literature:: In dichloromethane;
DOI:10.1021/jo000882k

Reference yield: 81.0%

: 167482-98-6
2,2′-((4-(tert-butyl)phenyl)methylene)bis(1H-pyrrole)

: 307930-88-7
S-2-pyridyl 4-tert-butylbenzothioate

: 307930-93-4
1-(4-tert-butylbenzoyl)-5-(4-tert-butylphenyl)dipyrromethane

Guidance literature:: 2,2′-((4-(tert-butyl)phenyl)methylene)bis(1H-pyrrole); With ethylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 0.166667h;

S-2-pyridyl 4-tert-butylbenzothioate; In tetrahydrofuran; for 0.5h; Further stages.;
DOI:10.1021/jo000882k

Reference yield:

: 307930-88-7
S-2-pyridyl 4-tert-butylbenzothioate

: 307931-01-7
1-(4-tert-butylbenzoyl)-5-(4-tert-butylphenyl)-9-(4-iodobenzoyl)dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: EtMgBr / tetrahydrofuran / 0.17 h / 20 °C

1.2: 81 percent / tetrahydrofuran / 0.5 h

2.1: EtMgBr / toluene; tetrahydrofuran / 0.08 h / 20 °C

2.2: 76 percent / toluene / 20 °C

With ethylmagnesium bromide; In tetrahydrofuran; toluene; 1.1: Metallation / 1.2: Acylation / 2.1: Metallation / 2.2: Acylation;
DOI:10.1021/jo000882k