Technology Process of 9H-Fluorene-2-carboxylic acid, 9-oxo-, methyl ester
There total 1 articles about 9H-Fluorene-2-carboxylic acid, 9-oxo-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Na2CO3 / Pd(OAc)2 / dimethylformamide; H2O / 12 h / 25 °C
2: MgSO4 / toluene / 100 °C
3: cesium pivalate / Pd(OAc)2; 1,1-bis(diphenylphosphino)methane / dimethylformamide / 12 h / 100 °C
4: aq. HCl / acetone
With
hydrogenchloride; sodium carbonate; magnesium sulfate; cesium pivalate;
palladium diacetate; bis-diphenylphosphinomethane;
In
water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ja070657l
- Guidance literature:
-
With
cesium fluoride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 48h;
Irradiation;
DOI:10.1039/c6ob01879c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether / 2 h / Heating
2: 92 percent / H2 / 10percent Pd/C / ethanol / 16 h / 760 Torr
With
lithium aluminium tetrahydride; hydrogen;
palladium on activated charcoal;
In
diethyl ether; ethanol;
