1,2-Cyclohexanedicarboxylic acid, 4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-, bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)-

Base Information

Chemical Name:1,2-Cyclohexanedicarboxylic acid, 4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-, bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)-
CAS No.:309761-65-7
Molecular Formula:C₂₆H₃₈O₈
Molecular Weight:478.583
Hs Code.:

1,2-Cyclohexanedicarboxylic acid,
4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-,
bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)-

Synonyms:

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Chemical Property of 1,2-Cyclohexanedicarboxylic acid, 4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-, bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)-

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,2-Cyclohexanedicarboxylic acid, 4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-, bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)-

There total 2 articles about 1,2-Cyclohexanedicarboxylic acid, 4-hydroxy-5-[(1R)-1-methyl-2-oxo-2-(phenylmethoxy)ethoxy]-, bis(1,1-dimethylethyl) ester, (1S,2S,4S,5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 93836-48-7
(S)-2-(trifluoromethanesulphonyloxy)propionic acid benzyl ester

: 221344-09-8
(1S,2S,4R,5S)-4,5-Dihydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester

: 309761-65-7
(1S,2S,4R,5S)-4-((R)-1-Benzyloxycarbonyl-ethoxy)-5-hydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester

Guidance literature:: (1S,2S,4R,5S)-4,5-Dihydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester; With di(n-butyl)tin oxide; In benzene; for 8h; Heating;

(S)-2-(trifluoromethanesulphonyloxy)propionic acid benzyl ester; With cesium fluoride; In 1,2-dimethoxyethane; for 4h; Further stages.;
DOI:10.1039/b210503a

Reference yield: 53.0%

: 93836-43-2
(R)-benzyl α-trifluoromethanesulphonyloxy propanoate

: 221344-09-8
(1S,2S,4R,5S)-4,5-Dihydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester

: 309761-65-7
(1S,2S,4R,5S)-4-((R)-1-Benzyloxycarbonyl-ethoxy)-5-hydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester

Guidance literature:: (1S,2S,4R,5S)-4,5-Dihydroxy-cyclohexane-1,2-dicarboxylic acid di-tert-butyl ester; With di(n-butyl)tin oxide; In benzene; Heating;

(R)-benzyl α-trifluoromethanesulphonyloxy propanoate; With tetra-(n-butyl)ammonium iodide; In benzene;
DOI:10.1016/S0960-894X(00)00428-5