Benzene, 1-chloro-2,3,5-trimethyl-

Base Information

• Chemical Name: Benzene, 1-chloro-2,3,5-trimethyl-
• CAS No.: 31053-98-2
• Molecular Formula: C₉H₁₁Cl
• Molecular Weight: 154.639
• Mol file: 31053-98-2.mol

Synonyms:Benzene,1-chloro-2,3,5-trimethyl;1-Chlor-2,3,5-trimethyl-benzol;1-chloro-2,3,5-trimethyl-benzene;

Chemical Property of Benzene, 1-chloro-2,3,5-trimethyl-

Chemical Property:

• Boiling Point: 215.0±9.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.029±0.06 g/cm3(Predicted)
• LogP: 3.26520

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzene, 1-chloro-2,3,5-trimethyl-

There total 3 articles about Benzene, 1-chloro-2,3,5-trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-3,4,6-trimethyl-aniline (872822-39-4) → 1-chloro-2,3,5-trimethyl-benzene (31053-98-2)

Guidance literature:

With phosphoric acid; sulfuric acid; Diazotization_.Behandlung der Diazoniumsalz-Loesung mit Aethanol und Kupfer-Pulver auf dem Dampfbad;

DOI:10.1021/ja01292a001

Reference yield:

2,4,5-trimethylaniline (137-17-7) → 1-chloro-2,3,5-trimethyl-benzene (31053-98-2)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine; ethanol; chloroform; chlorine

2: aqueous H₂SO₄; H₃PO₄ / Diazotization_.Behandlung der Diazoniumsalz-Loesung mit Aethanol und Kupfer-Pulver auf dem Dampfbad

With ethanol; chloroform; phosphoric acid; sulfuric acid; iodine; chlorine;

DOI:10.1021/ja01292a001

Reference yield:

→ 1-chloro-2,3,5-trimethyl-benzene (31053-98-2)

Guidance literature:

With copper(l) chloride;

upstream raw materials:

2-chloro-3,4,6-trimethyl-aniline

2,4,5-trimethylaniline