(2-PYRIDIN-4-YL-THIAZOL-4-YL)-ACETIC ACID

Base Information

• Chemical Name: (2-PYRIDIN-4-YL-THIAZOL-4-YL)-ACETIC ACID
• CAS No.: 31112-92-2
• Molecular Formula: C₁₀H₈N₂O₂S
• Molecular Weight: 220.252
• Mol file: 31112-92-2.mol

Synonyms:(2-Pyridin-4-yl-thiazol-4-yl)-acetic acid;2-(4-Pyridyl)-thiazol-4-yl-essigsaeure;

Chemical Property of (2-PYRIDIN-4-YL-THIAZOL-4-YL)-ACETIC ACID

Chemical Property:

• Melting Point: 248 - 249 °C
• PSA: 91.32000
• LogP: 1.83220

Purity/Quality:

98%min ^*data from raw suppliers

(2-Pyridin-4-yl-thiazol-4-yl)-acetic acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi,Xn
• Statements: 22

MSDS Files:

Useful:

Technology Process of (2-PYRIDIN-4-YL-THIAZOL-4-YL)-ACETIC ACID

There total 3 articles about (2-PYRIDIN-4-YL-THIAZOL-4-YL)-ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-(2-(pyridin-4-yl)thiazol-4-yl)acetate (578019-61-1) → (2-pyridin-4-yl-thiazol-4-yl)-acetic acid (31112-92-2)

Guidance literature:

With lithium hydroxide; In methanol; at 75 ℃; for 2h;

DOI:10.1016/j.bmcl.2007.07.045

Reference yield:

pyridine-4-carbothioamide (2196-13-6) → (2-pyridin-4-yl-thiazol-4-yl)-acetic acid (31112-92-2)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 12 h / Heating

2: aq. LiOH / methanol / 2 h / 75 °C

With lithium hydroxide; In methanol;

DOI:10.1016/j.bmcl.2007.07.045

Reference yield:

→ (2-pyridin-4-yl-thiazol-4-yl)-acetic acid (31112-92-2)

Guidance literature:

entspr.Ester,KOH;

upstream raw materials:

methyl 2-(2-(pyridin-4-yl)thiazol-4-yl)acetate

pyridine-4-carbothioamide

Downstream raw materials:

C₁₈H₁₅N₃O₃S

C₂₃H₁₇N₃O₂S

C₁₈H₁₅N₃O₂S

C₁₇H₁₂N₄OS

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