N,N-Dibenzylsulfamoyl chloride

Base Information

Chemical Name:N,N-Dibenzylsulfamoyl chloride
CAS No.:31367-40-5
Molecular Formula:C14H14ClNO2S
Molecular Weight:295.79
Hs Code.:
DSSTox Substance ID:DTXSID50538065
Nikkaji Number:J918.903C
Wikidata:Q82413284
Mol file:31367-40-5.mol

Synonyms:N,N-Dibenzylsulfamoyl chloride;31367-40-5;Dibenzylsulfamoyl chloride;Dibenzylsulfamyl chloride;N,N-Dibenzylsulfamoylchloride;SCHEMBL11594823;DTXSID50538065;CS-0351970;EN300-1612007

Suppliers and Price of N,N-Dibenzylsulfamoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N-Dibenzylsulfamoyl chloride

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:295.0433776
Heavy Atom Count:19
Complexity:334

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN(CC2=CC=CC=C2)S(=O)(=O)Cl

Technology Process of N,N-Dibenzylsulfamoyl chloride

There total 1 articles about N,N-Dibenzylsulfamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 103-49-1
dibenzylamine

: 31367-40-5
dibenzylsulfamoyl chloride

Guidance literature:: With sulfuryl dichloride; triethylamine; In Petroleum ether; for 1h; Ambient temperature;

Reference yield: 40.0%

: 106-41-2
4-bromo-phenol

: 31367-40-5
dibenzylsulfamoyl chloride

: 1400942-66-6
4-bromophenyl dibenzylsulfamate

Guidance literature:: With caesium carbonate; In tetrahydrofuran; at 67 ℃; for 16h;
DOI:10.1039/c2ob26057c

Reference yield:

: 106-41-2
4-bromo-phenol

: 31367-40-5
dibenzylsulfamoyl chloride

: 1400942-41-7
[1,1′-biphenyl]-4-yl dibenzylsulfamate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / tetrahydrofuran / 16 h / 67 °C

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; caesium carbonate; In tetrahydrofuran; acetonitrile; 2: |Suzuki Coupling;
DOI:10.1039/c2ob26057c