Thieno[3,2-b]quinoline-4(2H)-carboxylic acid, 9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-, 1,1-dimethylethyl ester, 1,1-dioxide

Base Information

Chemical Name:Thieno[3,2-b]quinoline-4(2H)-carboxylic acid, 9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-, 1,1-dimethylethyl ester, 1,1-dioxide
CAS No.:315188-33-1
Molecular Formula:C22H23BrFNO5S
Molecular Weight:512.397
Hs Code.:

Thieno[3,2-b]quinoline-4(2H)-carboxylic acid,
9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-,
1,1-dimethylethyl ester, 1,1-dioxide

Synonyms:

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Chemical Property of Thieno[3,2-b]quinoline-4(2H)-carboxylic acid, 9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-, 1,1-dimethylethyl ester, 1,1-dioxide

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Technology Process of Thieno[3,2-b]quinoline-4(2H)-carboxylic acid, 9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-, 1,1-dimethylethyl ester, 1,1-dioxide

There total 3 articles about Thieno[3,2-b]quinoline-4(2H)-carboxylic acid, 9-(3-bromo-4-fluorophenyl)-3,5,6,7,8,9-hexahydro-8-oxo-, 1,1-dimethylethyl ester, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5220-49-5
3-amino-cyclohex-2-enone

: 315188-33-1
1,1-dimethylethyl 9-(3-bromo-4-fluorophenyl)-8-oxo-3,5,6,7,8,9-hexahydrothieno[3,2-b]quinoline-4(2H)-carboxylate 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 10.56 g / ethanol / 72 h / Heating

2: 900 mg / DMAP / acetonitrile / 1 h / Heating

With dmap; In ethanol; acetonitrile;
DOI:10.1021/jm030356w

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 315188-33-1
1,1-dimethylethyl 9-(3-bromo-4-fluorophenyl)-8-oxo-3,5,6,7,8,9-hexahydrothieno[3,2-b]quinoline-4(2H)-carboxylate 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 10.56 g / ethanol / 72 h / Heating

2: 900 mg / DMAP / acetonitrile / 1 h / Heating

With dmap; In ethanol; acetonitrile;
DOI:10.1021/jm030356w