3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl

Base Information

Chemical Name:3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl
CAS No.:31590-68-8
Molecular Formula:C₂₈H₄₂
Molecular Weight:378.641
Hs Code.:
DSSTox Substance ID:DTXSID80506772
Nikkaji Number:J1.307.020B
Wikidata:Q82362683
Mol file:31590-68-8.mol

Synonyms:31590-68-8;DTXSID80506772;3,3',5,5'-tetra-t-butylbiphenyl;3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl

Suppliers and Price of 3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl

Chemical Property:

PSA：0.00000
LogP:8.54360
XLogP3:10.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:378.328651340
Heavy Atom Count:28
Complexity:406

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=CC(=C1)C2=CC(=CC(=C2)C(C)(C)C)C(C)(C)C)C(C)(C)C

Technology Process of 3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl

There total 1 articles about 3,3',5,5'-Tetra-tert-butyl-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 529-28-2
4-iodoanisol

: 22385-77-9
1-bromo-3,5-di-tert-butylbenzene

: 4877-93-4
2,2'-Dimethoxybiphenyl

: 31590-68-8
3,3’,5,5’-tetra-tert-butylbiphenyl

: 3',5'-di-tert-butyl-2-methoxy-1,1'-biphenyl

Guidance literature:: With bis(tri-tert-butylphosphine)palladium⁽⁰⁾; (C₅H₅)2Zr(OC₄H₈)N(Si(CH₃)3)CH(C₆H₅); tri-tert-butyl phosphine; In toluene; at 80 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.chempr.2021.06.007