2,3,6,7-Anthracenetetrol

Base Information

Chemical Name:2,3,6,7-Anthracenetetrol
CAS No.:3178-75-4
Molecular Formula:C14H10O4
Molecular Weight:242.231
Hs Code.:
Mol file:3178-75-4.mol

Synonyms:Anthracene-2,3,6,7-tetraol;2,3,6,7-Tetrahydroxy-anthracen;

Suppliers and Price of 2,3,6,7-Anthracenetetrol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 15 raw suppliers

Chemical Property of 2,3,6,7-Anthracenetetrol

Chemical Property:

Melting Point:325 - 335 °C
PSA：80.92000
LogP:2.81540

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2,3,6,7-Anthracenetetrol

There total 10 articles about 2,3,6,7-Anthracenetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 93878-11-6
2,3,6,7-tetramethoxylanthracene

: 3178-75-4
2,3,6,7-tetrahydroxyanthracene

Guidance literature:: With boron tribromide; In dichloromethane; for 2h; Heating;
DOI:10.1021/ja036466+

Reference yield:

: 5629-55-0
2,3,6,7-tetramethoxy-9,10-anthraquinone

: 3178-75-4
2,3,6,7-tetrahydroxyanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / tetra-n-butylammonium borohydride; iodomethane / CH₂Cl₂ / 0 - 20 °C

2: 85 percent / conc. HBr; tetra-n-butylammonium bromide / Heating

With tetra(n-butyl)ammonium borohydride; tetrabutylammomium bromide; hydrogen bromide; methyl iodide; In dichloromethane;
DOI:10.1016/j.tet.2004.07.017

Reference yield:

: 140648-13-1
9,10-diethyl-2,3,6,7-tetramethoxy-anthracene

: 3178-75-4
2,3,6,7-tetrahydroxyanthracene

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / K₂Cr₂O₇; acetic acid / 0.5 h / 90 °C

2: 89 percent / H₂; acetic acid / Pd/C / 0.75 h / 90 °C

3: 69 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 20 °C

4: 97 percent / BBr₃ / CH₂Cl₂ / 2 h / Heating

With potassium dichromate; lithium aluminium tetrahydride; hydrogen; boron tribromide; acetic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja036466+