Technology Process of (2-Iodoethenylidene)cyclohexane
There total 3 articles about (2-Iodoethenylidene)cyclohexane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 86 percent / Cuprous bromide, ammonium bromide, copper powder / HBr / 1.5 h / 0 °C
2: 1.) n-butyllithium; 2.) 1,2-diiodoethane / 1.) Ether, hexane, -78 deg C, 30 min; 2.) 0 deg C, 1 h; Room temperature, 10 minute
With
n-butyllithium; ammonium bromide; 1,2-Diiodoethane; copper; copper(I) bromide;
In
hydrogen bromide;
DOI:10.1021/jo01308a013
- Guidance literature:
-
Multistep reaction;
(i) Me2CuLi, Et2O, (ii) I2, 1,2-dimethoxy-ethane;
DOI:10.1039/c39770000761
- Guidance literature:
-
With
n-butyllithium; 1,2-Diiodoethane;
Yield given. Multistep reaction;
1.) Ether, hexane, -78 deg C, 30 min; 2.) 0 deg C, 1 h; Room temperature, 10 minute;
DOI:10.1021/jo01308a013
