1,4-Bis(n-propylaminomethyl)benzene dihydrochloride

Base Information

Chemical Name:1,4-Bis(n-propylaminomethyl)benzene dihydrochloride
CAS No.:93865-87-3
Molecular Formula:C14H24 N2 . 2 Cl H
Molecular Weight:293.2756
Hs Code.:
DSSTox Substance ID:DTXSID50239823

Synonyms:1,4-Bis(n-propylaminomethyl)benzene dihydrochloride;p-Xylene-alpha,alpha'-diamine, N,N'-dipropyl-, dihydrochloride;N,N'-Dipropyl-p-xylene-alpha,alpha'-diamine dihydrochloride;93865-87-3;DTXSID50239823;LS-162596

Suppliers and Price of 1,4-Bis(n-propylaminomethyl)benzene dihydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1,4-Bis(n-propylaminomethyl)benzene dihydrochloride

Chemical Property:

Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:292.1473042
Heavy Atom Count:18
Complexity:133

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCNCC1=CC=C(C=C1)CNCCC.Cl.Cl

Technology Process of 1,4-Bis(n-propylaminomethyl)benzene dihydrochloride

There total 4 articles about 1,4-Bis(n-propylaminomethyl)benzene dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1377583-14-6
N,N'-dipropyl-N,N'-di-Boc-p-xylylenediamine

: 93865-87-3
N,N'-dipropyl-p-xylylenediammonium chloride

Guidance literature:: With hydrogenchloride; In ethanol; water; at 20 ℃; for 16h;
DOI:10.1002/chem.201103434

Reference yield:

: 539-48-0
p-xylylidenediamine

: 93865-87-3
N,N'-dipropyl-p-xylylenediammonium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / methanol; water

2.1: triethylamine / 20 °C

2.2: 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: hydrogenchloride / ethanol; water / 16 h / 20 °C

With hydrogenchloride; sodium hydride; triethylamine; In methanol; ethanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201103434

Reference yield:

: 51964-30-8,3057-45-2,116599-23-6
1,4-bis(aminomethyl)benzene dihydrochloride

: 93865-87-3
N,N'-dipropyl-p-xylylenediammonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 20 °C

1.2: 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: hydrogenchloride / ethanol; water / 16 h / 20 °C

With hydrogenchloride; sodium hydride; triethylamine; In ethanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/chem.201103434