Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-

Base Information

Chemical Name:Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-
CAS No.:14796-86-2
Molecular Formula:C24H19 N2 O2 P
Molecular Weight:398.3936
Hs Code.:2931900090
NSC Number:165770
DSSTox Substance ID:DTXSID60304430
Nikkaji Number:J128.809A
Wikidata:Q82050333
Mol file:14796-86-2.mol

Synonyms:14796-86-2;Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-;N-(3-Nitrophenyl)triphenylphosphine imide;(3-nitrophenyl)imino-triphenyl-lambda5-phosphane;3-Nitro-N-(triphenylphosphoranylidene)aniline;NSC165770;Phosphine imide, N-(m-nitrophenyl)-P,P,P-triphenyl-;DTXSID60304430;AGFAUKFPPPZZIA-UHFFFAOYSA-N;AKOS001031930;NSC-165770;(3-nitrophenylimino)triphenylphosphorane;FT-0704758;[(3-Nitrophenyl)imino](triphenyl)phosphorane #;Z56762327;N-(3-NITROPHENYL)-P,P,P-TRIPHENYLPHOSPHINE IMIDE;N-(3-NITROPHENYL)-111-TRIPHENYL-LAMBDA5-PHOSPHANIMINE

Suppliers and Price of Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-(3-NITROPHENYL)-P,P,P-TRIPHENYLPHOSPHINE IMIDE Aldrich
250mg
$ 144.00

American Custom Chemicals Corporation
N1-(1,1,1-TRIPHENYL-LAMBDA5-PHOSPHANYLIDENE)-3-NITROANILINE 95.00%
5MG
$ 496.53

Total 4 raw suppliers

Chemical Property of Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-

Chemical Property:

Vapor Pressure:3.24E-12mmHg at 25°C
Boiling Point:565.3°Cat760mmHg
Flash Point:295.7°C
PSA：67.99000
Density:1.18g/cm³
LogP:5.92720
XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:398.11841485
Heavy Atom Count:29
Complexity:532

Purity/Quality:

99% ^*data from raw suppliers

N-(3-NITROPHENYL)-P,P,P-TRIPHENYLPHOSPHINE IMIDE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=NC2=CC(=CC=C2)[N+](=O)[O-])(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)-

There total 4 articles about Benzenamine, 3-nitro-N-(triphenylphosphoranylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 603-35-0
triphenylphosphine

: 99-09-2
3-nitro-aniline

: 14796-86-2
N-(3-nitrophenyl)triphenylphosphine imine

Guidance literature:: With hexachloroethane; triethylamine; In acetonitrile; at 20 ℃;
DOI:10.1107/S0108270109047763

Reference yield:

: 603-35-0
triphenylphosphine

: 14796-86-2
N-(3-nitrophenyl)triphenylphosphine imine

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂ / CCl₄

2: Et₃N / CCl₄ / 2 h / Heating

With bromine; triethylamine; In tetrachloromethane; 1: Bromination / 2: Condensation;