1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol

Base Information

Chemical Name:1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol
CAS No.:32469-38-8
Molecular Formula:C13H22O3
Molecular Weight:226.316
Hs Code.:
DSSTox Substance ID:DTXSID10575971
Wikidata:Q82465465

Synonyms:32469-38-8;SCHEMBL9782753;DTXSID10575971;1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol

Suppliers and Price of 1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:226.15689456
Heavy Atom Count:16
Complexity:323

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC(CC(C1(C#CC(C)O)O)(C)C)O

Technology Process of 1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol

There total 1 articles about 1-(3-Hydroxybut-1-yn-1-yl)-2,2,6-trimethylcyclohexane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32469-38-8
4-(1,4-dihydroxy-2,2,6-trimethylcyclohexyl)-3-butyn-2-ol

Guidance literature:: 4-Oxoverb. 3, NaBH4-Red.;

Reference yield: 78.0%

: 32469-38-8,125810-91-5
(3RS,5RS,6SR,9SR)-megastigm-7-yne-3,6,9-triol

: 23726-93-4
Damascenon

: 35734-61-3,56915-02-7
3-hydroxymegastigma-5,8-dien-7-one

: 41436-47-9
9-hydroxymegastigma-3,5-dien-7-one

: 125791-43-7
3-Hydroxy-1-(4-hydroxy-2,6,6-trimethyl-cyclohex-1-enyl)-butan-1-one

Guidance literature:: With sulfuric acid; In ethanol; water; at 100 ℃; for 1.33h; Product distribution; var. reaction times, temperatures; also for megastigm-5-en-7-yne-3,9-diol ⁽¹⁰⁾;

Reference yield:

: 32469-38-8
4-(1,4-dihydroxy-2,2,6-trimethylcyclohexyl)-3-butyn-2-ol

: 144-68-3
zeaxanthin

Guidance literature:: Multi-step reaction with 4 steps

1: 3.5 g / lithium aluminium hydride / tetrahydrofuran / 3 h / Heating

2: 2.21 g / CHCl₃ / 18 h / 20 °C

3: 11 mg / aq. KOH / propan-2-ol / 24 h / 20 °C

4: 8.5 mg / aq. KOH / propan-2-ol / 3 h / 20 °C

With potassium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; chloroform; isopropyl alcohol;
DOI:10.1002/hlca.19810640414