1-Butanethiol,mercury(2+) salt (8CI,9CI)

Base Information

• Chemical Name: 1-Butanethiol,mercury(2+) salt (8CI,9CI)
• CAS No.: 23601-34-5
• Molecular Formula: C₈H₁₈HgS₂
• Molecular Weight: 378.953
• Mol file: 23601-34-5.mol

Synonyms:Bis(1-butanethiolato)mercury;Bis(butylthio)mercury; Mercury, bis(1-butanethiolato-S)-

Chemical Property of 1-Butanethiol,mercury(2+) salt (8CI,9CI)

Chemical Property:

• Boiling Point: 98.2°Cat760mmHg
• Flash Point: 12.8°C
• Density: 0.83g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Butanethiol,mercury(2+) salt (8CI,9CI)

There total 4 articles about 1-Butanethiol,mercury(2+) salt (8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.3%

n-butanethiol (109-79-5) + mercury(II) nitrate → bis(1-butanethiolato)mercury(II) (23601-34-5)

Guidance literature:

In ethanol; water; the thiol was added to soln. of Hg(NO3)2 in EtOH/H2O in a Schlenk tube; soln. was stirred for 12 h in the dark; ppt. was filtered off, washed with cold EtOH and dried in vacuo;

DOI:10.1021/ic000638b

Reference yield: 66.0%

n-butanethiol (109-79-5) + mercury(II) iodide → bis(1-butanethiolato)mercury(II) (23601-34-5)

Guidance literature:

With triethylamine; In ethanol; byproducts: triethylammonium iodide; the thiol was added to soln. of HgI2 in EtOH in a Schlenk tube; Et3N wasadded; ppt. was filtered off, washed with water and dried in vacuo;

DOI:10.1021/ic000638b

Reference yield:

n-butanethiol (109-79-5) + mercury → bis(1-butanethiolato)mercury(II) (23601-34-5)

Guidance literature:

In acetonitrile; Electrochem. Process; electrochem. oxidation of anodic Hg in CH3CN soln. of ligand for 5 h at15 V, in the presence of (C2H5)4NClO4; soln. was decanted, collected, washed with CH3CN and petroleum ether, dried; elem. anal.;

DOI:10.1016/S0020-1693(00)87298-9

upstream raw materials:

n-butanethiol

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