5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine

Base Information

Chemical Name:5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine
CAS No.:2064-28-0
Molecular Formula:C16H16N2
Molecular Weight:236.3116
Hs Code.:
DSSTox Substance ID:DTXSID20174676
Nikkaji Number:J1.552.937G

Synonyms:5-(2-AMINOETHYL)-5H-DIBENZO(B,F)AZEPINE;2064-28-0;5-(2-Aminoethyl)-5H-dibenzo[b,f]azepine;DTXSID20174676;5H-Dibenz[b,f]azepine-5-ethanamine

Suppliers and Price of 5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine

Chemical Property:

Vapor Pressure:1.09E-06mmHg at 25°C
Boiling Point:402.6°Cat760mmHg
Flash Point:174.2°C
Density:1.128g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:236.131348519
Heavy Atom Count:18
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=CC=CC=C3N2CCN

Technology Process of 5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine

There total 3 articles about 5-(2-Aminoethyl)-5H-dibenzo(B,F)azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1262142-21-1
N-(2-(5H-dibenzo[b,f]azepin-5-yl)ethyl)-2,2,2-trifluoroacetamide

: 2064-28-0
5-(aminoethyl)dibenzazepine

Guidance literature:: With water; potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/acschemneuro.8b00242

Reference yield:

: 244059-01-6
5-(cyanomethyl)dibenzazepine

: 2064-28-0
5-(aminoethyl)dibenzazepine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jm9811155

Reference yield:

: 256-96-2
dibenzoazepine

: 2064-28-0
5-(aminoethyl)dibenzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / Na₂CO₃ / CH₂Cl₂ / 168000 h / Heating

2: LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm040768k