Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)-

Base Information

Chemical Name:Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)-
CAS No.:3286-88-2
Molecular Formula:C13H9BrO3
Molecular Weight:293.11300
Hs Code.:

Synonyms:4'-Brom-2,4-dihydroxy-benzophenon;(4-bromo-phenyl)-(2,4-dihydroxyphenyl)-methanone;4'-bromo-2,4-dihydroxy-benzophenone;(4-Bromo-phenyl)-(2,4-dihydroxy-phenyl)-methanone;

Suppliers and Price of Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)-

Chemical Property:

Melting Point:169 °C
PSA：57.53000
LogP:3.09130

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)-

There total 5 articles about Methanone, (4-bromophenyl)(2,4-dihydroxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 500293-60-7
(4-bromophenyl)(2,4-dimethoxyphenyl)methanone

: 3286-88-2
(4-bromophenyl)(2,4-dihydroxyphenyl)methanone

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 46h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201903472

Reference yield:

: 151-10-0
1,3-Dimethoxybenzene

: 3286-88-2
(4-bromophenyl)(2,4-dihydroxyphenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: AlCl₃ / nitrobenzene / 0.17 h / 0 - 8 °C

1.2: nitrobenzene / 6 - 20 °C

2.1: aq. HBr; AcOH / 5 h / Heating

With aluminium trichloride; hydrogen bromide; acetic acid; In nitrobenzene;
DOI:10.1021/jm021120f

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 3286-88-2
(4-bromophenyl)(2,4-dihydroxyphenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: AlCl₃ / nitrobenzene / 0.17 h / 0 - 8 °C

1.2: nitrobenzene / 6 - 20 °C

2.1: aq. HBr; AcOH / 5 h / Heating

With aluminium trichloride; hydrogen bromide; acetic acid; In nitrobenzene;
DOI:10.1021/jm021120f