[1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER

Base Information

Chemical Name:[1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER
CAS No.:330551-18-3
Molecular Formula:C15H23N3O2
Molecular Weight:277.36200
Hs Code.:2933990090
Mol file:330551-18-3.mol

Synonyms:1-Ethyl-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)urea;[1-(4-aminophenyl)pyrrolidin-3-yl]carbamic acid tert-butyl ester;3-(tert-butoxycarbonylamino)-1-(4-aminophenyl)pyrrolidine;[(4-ethylureido)phenyl]boronic acid pinacol ester;4-(3-Ethylureido)benzeneboronic acid,pinacol ester;4-(3-ethylureido)phenyl boronic acid pinacol ester;[4-(3-tert-butoxycarbonylaminopyrrolidin-1-yl)phenyl]amine;tert-butyl 1-(4-aminophenyl)pyrrolidin-3-ylcarbamate;

Suppliers and Price of [1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
[1-(4-amino-phenyl)-pyrrolidin-3-yl]-carbamicacidtert-butylester 95
5g
$ 1633.00

American Custom Chemicals Corporation
[1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER 95.00%
5MG
$ 501.23

Total 2 raw suppliers

Chemical Property of [1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER

Chemical Property:

PSA：71.08000
LogP:3.22280

Purity/Quality:

98% ^*data from raw suppliers

[1-(4-amino-phenyl)-pyrrolidin-3-yl]-carbamicacidtert-butylester 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER

There total 3 articles about [1-(4-AMINO-PHENYL)-PYRROLIDIN-3-YL]-CARBAMIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99724-19-3,140629-77-2
3-(tert-butoxycarbonylamino)pyrrolidine

: 330551-18-3
[1-(4-aminophenyl)pyrrolidin-3-yl]carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-diisopropylethylamine / acetonitrile / 14 h / Heating

2: H₂ / Ra-Ni / tetrahydrofuran / 5 h / 20 °C / 2585.74 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; Ra-Ni; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm049355+

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 330551-18-3
[1-(4-aminophenyl)pyrrolidin-3-yl]carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-diisopropylethylamine / acetonitrile / 14 h / Heating

2: H₂ / Ra-Ni / tetrahydrofuran / 5 h / 20 °C / 2585.74 Torr

With hydrogen; N-ethyl-N,N-diisopropylamine; Ra-Ni; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm049355+