ASISCHEM V97345

Base Information

Chemical Name:ASISCHEM V97345
CAS No.:332922-15-3
Molecular Formula:C17H14FNO
Molecular Weight:267.29800
Hs Code.:2933990090
Mol file:332922-15-3.mol

Synonyms:

Suppliers and Price of ASISCHEM V97345

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-[(4-FLUOROPHENYL)METHYL]-2-METHYL-1H-INDOLE-3-CARBOXALDEHYDE 95.00%
5MG
$ 497.54

Total 3 raw suppliers

Chemical Property of ASISCHEM V97345

Chemical Property:

Vapor Pressure:1.61E-08mmHg at 25°C
Boiling Point:456.5oC at 760 mmHg
Flash Point:229.9oC
PSA：22.00000
Density:1.15g/cm3
LogP:3.94960

Purity/Quality:

99% ^*data from raw suppliers

1-[(4-FLUOROPHENYL)METHYL]-2-METHYL-1H-INDOLE-3-CARBOXALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ASISCHEM V97345

There total 3 articles about ASISCHEM V97345 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5416-80-8
2-methyl-1H-indole-3-carbaldehyde

: 352-11-4
1-chloromethyl-4-fluorobenzene

: 332922-15-3
1-(4-fluorobenzyl)-3-formyl-2-methyl-1H-indole

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1016/S0223-5234(02)00005-3

Reference yield: 75.0%

: 332922-15-3
1-(4-fluorobenzyl)-3-formyl-2-methyl-1H-indole

Guidance literature:

Reference yield:

: 95-20-5
2-methyl-1H-indole

: 332922-15-3
1-(4-fluorobenzyl)-3-formyl-2-methyl-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorus oxychloride / 2 h / 5 - 20 °C

1.2: 90 percent / potassium hydroxide / H₂O

2.1: 75 percent / NaH / dimethylsulfoxide / 2 h / 20 °C

With sodium hydride; trichlorophosphate; In dimethyl sulfoxide; 1.1: Vilsmeier-Haack reaction;
DOI:10.1016/S0223-5234(02)00005-3