2-Buten-1-ol, 2-methyl-, acetate

Base Information

Chemical Name:2-Buten-1-ol, 2-methyl-, acetate
CAS No.:33425-30-8
Molecular Formula:C₇H₁₂O₂
Molecular Weight:128.171
Hs Code.:

Synonyms:2-Methyl-trans-crotylaldehyd-acetat;1-Acetoxy-2-methyl-buten-2;2-Buten-1-ol,2-methyl-,acetate;2-Methyl-trans-but-2-en-1-yl Acetat;

Suppliers and Price of 2-Buten-1-ol, 2-methyl-, acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Buten-1-ol, 2-methyl-, acetate

Chemical Property:

PSA：57.53000
LogP:1.03580

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Buten-1-ol, 2-methyl-, acetate

There total 5 articles about 2-Buten-1-ol, 2-methyl-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 497-02-9
(E)-2-methyl-2-buten-1-ol

: 108-24-7
acetic anhydride

: 33425-30-8,41414-68-0,19248-94-3
Essigsaeure-<(E)-2-methyl-2-butenyl>ester

Guidance literature:: With pyridine; at 25 ℃; for 12h;
DOI:10.1002/hlca.19800630516

Reference yield:

: 10473-14-0
3-methyl-3-buten-2-ol

: 33425-30-8,41414-68-0,19248-94-3
Essigsaeure-<(E)-2-methyl-2-butenyl>ester

Guidance literature:: Multi-step reaction with 2 steps

1: Py

2: (isomerization)

With pyridine;
DOI:10.1021/ja01005a020

Reference yield:

: 497-03-0
2-methylbut-2-enal

: 33425-30-8,41414-68-0,19248-94-3
Essigsaeure-<(E)-2-methyl-2-butenyl>ester

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / LiAlH₄ / diethyl ether / 1.5 h / Ambient temperature

2: 87 percent / pyridine, p-(dimethylamino)pyridine / Ambient temperature

With pyridine; dmap; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jf9508209