Tris(4-methylphenyl)germane

Base Information

Chemical Name:Tris(4-methylphenyl)germane
CAS No.:3351-47-1
Molecular Formula:C21H22Ge
Molecular Weight:346.996
Hs Code.:
DSSTox Substance ID:DTXSID50783730

Synonyms:Tris(4-methylphenyl)germane;3351-47-1;DTXSID50783730

Suppliers and Price of Tris(4-methylphenyl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Tris(4-methylphenyl)germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:347.0855034
Heavy Atom Count:22
Complexity:263

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)[Ge](C2=CC=C(C=C2)C)C3=CC=C(C=C3)C

Technology Process of Tris(4-methylphenyl)germane

There total 2 articles about Tris(4-methylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-43-4
para-chlorotoluene

: 3351-47-1
tri(p-tolyl)germane

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / tetrahydrofuran

2: diethyl ether

With Mg; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.jorganchem.2006.03.049

Reference yield:

: 3351-47-1
tri(p-tolyl)germane

Guidance literature:: aus p-Tolylmagnesiumbromid;
DOI:10.1021/ic50108a009

Reference yield: 80.0%

: 109-72-8,29786-93-4
n-butyllithium

: 3351-47-1
tri(p-tolyl)germane

: 103457-87-0
Brom-di-tert-butylmethylsilan

: 926312-90-5
tert-Bu₂MeSiGe(p-tolyl)3

Guidance literature:: In tetrahydrofuran; diethyl ether; hexane; (inert conditions); addn. of soln. of BuLi in hexane to soln. of germanium compd. in ether, stirring at room temp. for 1 h, addn. to soln. of silane deriv. in THF, stirring overnight at room temp.; usual work up, Kugelrohr distillation, NMR;
DOI:10.1016/j.jorganchem.2006.03.049