9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester

Base Information

Chemical Name:9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester
CAS No.:33821-71-5
Molecular Formula:C15H14N2O2
Molecular Weight:254.28400
Hs Code.:
DSSTox Substance ID:DTXSID60458104
Nikkaji Number:J3.440.200K
Wikidata:Q82281248

Synonyms:33821-71-5;9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester;SCHEMBL2216825;DTXSID60458104;1-Methyl-beta-carboline-3-carboxylic acid ethyl ester

Suppliers and Price of 9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester

Chemical Property:

PSA：54.98000
LogP:3.20120
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:254.105527694
Heavy Atom Count:19
Complexity:347

Purity/Quality:: 99%+, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=NC(=C2C(=C1)C3=CC=CC=C3N2)C

Technology Process of 9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester

There total 20 articles about 9H-Pyrido[3,4-b]indole-3-carboxylic acid, 1-methyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 84543-27-1
ethyl 9-methoxymethyl-1-methylpyrido<3,4-b>indole-3-carboxylate

: 33821-71-5
ethyl 1-methyl-9H-pyrido[3,4-b]indole-3-carboxylateyl-2,3,4,9-tetrahydro-1Hpyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With formic acid; for 5h; Heating;

Reference yield: 81.0%

: 33821-71-5
ethyl 1-methyl-9H-pyrido[3,4-b]indole-3-carboxylateyl-2,3,4,9-tetrahydro-1Hpyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With sulfur; In 5,5-dimethyl-1,3-cyclohexadiene; for 10h; Reflux;

Reference yield: 79.0%

: 39824-90-3
ethyl 1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate

: 33821-71-5
ethyl 1-methyl-9H-pyrido[3,4-b]indole-3-carboxylateyl-2,3,4,9-tetrahydro-1Hpyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(ll) bromide; In dimethyl sulfoxide; at 25 ℃; for 16h; Green chemistry;
DOI:10.1039/c7ra13434g