Technology Process of 3-Methylhexadecanoic acid
There total 5 articles about 3-Methylhexadecanoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dicyclohexylamine, nBuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 3 h, 2.) -25 deg C, 1 h
2: 1.) H2, 2.) KOH / 1.) Pt / 1.) EtOH, 2.) EtOH, H2O, 8 h, reflux
With
potassium hydroxide; n-butyllithium; hydrogen; N-cyclohexyl-cyclohexanamine;
platinum;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 81 percent / ethyl acetate / 5 h / Heating
2: Dicyclohexylamine, nBuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 3 h, 2.) -25 deg C, 1 h
3: 1.) H2, 2.) KOH / 1.) Pt / 1.) EtOH, 2.) EtOH, H2O, 8 h, reflux
With
potassium hydroxide; n-butyllithium; hydrogen; N-cyclohexyl-cyclohexanamine;
platinum;
In
tetrahydrofuran; hexane; ethyl acetate;
- Guidance literature:
-
With
potassium hydroxide; hydrogen;
platinum;
Yield given. Multistep reaction;
1.) EtOH, 2.) EtOH, H2O, 8 h, reflux;
