Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-

Base Information

Chemical Name:Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-
CAS No.:339320-26-2
Molecular Formula:C17H17BrO3
Molecular Weight:349.224
Hs Code.:
DSSTox Substance ID:DTXSID00475976
Wikidata:Q82306820

Synonyms:339320-26-2;Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-;DTXSID00475976

Suppliers and Price of Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:348.03611
Heavy Atom Count:21
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)C2=CC=C(C=C2)OCCCCBr)O

Technology Process of Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)-

There total 1 articles about Methanone, [4-(4-bromobutoxy)phenyl](4-hydroxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 110-52-1
1,4-dibromo-butane

: 611-99-4
4,4'-Dihydroxybenzophenone

: 339320-26-2
4-(4-Bromobutoxy)-4'-hydroxybenzophenone

Guidance literature:: 4,4'-Dihydroxybenzophenone; With potassium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

1,4-dibromo-butane; In tetrahydrofuran; N,N-dimethyl-formamide; Further stages.;
DOI:10.1039/b009553m

Reference yield: 62.0%

: 339320-27-3
cyclopentadienyltricarbonylrhenium ethyl ketone

: 339320-26-2
4-(4-Bromobutoxy)-4'-hydroxybenzophenone

: 339320-28-4,339320-30-8
C₅H₄Re(CO)3C₂H₅CCC₆H₄OHC₆H₄O(CH₂)4Br

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; TiCl4 mixed with Zn at o°C, refluxed for 2 h, cooled to room temp., mixed with Re complex and benzophenone, refluxed for 2 h, cooled to room temp.; stirred with H2O and CH2Cl2, MAS;
DOI:10.1039/b009553m

Reference yield: 46.0%

: propionylferrocene

: 339320-26-2
4-(4-Bromobutoxy)-4'-hydroxybenzophenone

: 401837-93-2
C₅H₅FeC₅H₄C(CH₂CH₃)C(C₆H₄O(CH₂)4Br)C₆H₄OH

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; under Ar; TiCl4 was added dropwise to a suspn. of Zn in THF at -10°C, mixt. was heated at reflux for 1.5 h, allowed to cool to room temp., ketone and complex were added dropwise, mixt. was heated for 2 h, cooled to room temp.; hydrolyzed with 10% K2CO3, extd. with ether, solvent was removed, chromy. (silica gel, Et2O/pentane);
DOI:10.1016/S0022-328X(01)00953-6