4,5-Acridinediamine

Base Information

• Chemical Name: 4,5-Acridinediamine
• CAS No.: 3407-96-3
• Molecular Formula: C13H11N3
• Molecular Weight: 209.25
• Mol file: 3407-96-3.mol

Synonyms:

Chemical Property of 4,5-Acridinediamine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,5-Acridinediamine

There total 5 articles about 4,5-Acridinediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4,5-diaminoacridine-9(10H)-one (89023-36-9) → 4,5-diaminoacridine (3407-96-3)

Guidance literature:

With sodium amalgam; water; at 80 ℃; for 2h;

DOI:10.1080/00304940009355954

Reference yield:

2-bromo-3-nitro-benzoic acid (573-54-6) → 4,5-diaminoacridine (3407-96-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 32 percent / Na₂CO₃; K₂CO₃; Cu / 3 h / 192 °C

2: 87 percent / H₂SO₄ / 1.5 h / 100 °C

3: 65 percent / aq. HCl; SnCl₂ / 3 h / Heating

4: 65 percent / 5 percent Na/Hg; H₂O / 2 h / 80 °C

With hydrogenchloride; sodium amalgam; sulfuric acid; water; copper; sodium carbonate; potassium carbonate; tin(ll) chloride;

DOI:10.1080/00304940009355954

Reference yield:

4,5-dinitro-9(10H)-acridinone (327185-81-9) → 4,5-diaminoacridine (3407-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / aq. HCl; SnCl₂ / 3 h / Heating

2: 65 percent / 5 percent Na/Hg; H₂O / 2 h / 80 °C

With hydrogenchloride; sodium amalgam; water; tin(ll) chloride;

DOI:10.1080/00304940009355954

upstream raw materials:

4,5-diaminoacridine-9(10H)-one

2-bromo-3-nitro-benzoic acid

4,5-dinitro-9(10H)-acridinone

2,2'-Dinitrodiphenylamine-6-carboxylic acid