4-Phenyl-3-buten-2-one (4-nitrophenyl)hydrazone

Base Information

• Chemical Name: 4-Phenyl-3-buten-2-one (4-nitrophenyl)hydrazone
• CAS No.: 34292-79-0
• Molecular Formula: C16H15N3O2
• Molecular Weight: 281.314
• European Community (EC) Number: 658-277-4

Synonyms:AKOS001334246;Z57069143;4-PHENYL-3-BUTEN-2-ONE (4-NITROPHENYL)HYDRAZONE;(2E)-1-(4-NITROPHENYL)-2-[(3E)-4-PHENYLBUT-3-EN-2-YLIDENE]HYDRAZINE

Chemical Property of 4-Phenyl-3-buten-2-one (4-nitrophenyl)hydrazone

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 281.116426730
• Heavy Atom Count: 21
• Complexity: 387

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC1=CC=C(C=C1)[N+](=O)[O-])C=CC2=CC=CC=C2
• Isomeric SMILES: C/C(=N\NC1=CC=C(C=C1)[N+](=O)[O-])/C=C/C2=CC=CC=C2

Technology Process of 4-Phenyl-3-buten-2-one (4-nitrophenyl)hydrazone

There total 2 articles about 4-Phenyl-3-buten-2-one (4-nitrophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophenylhydrazine hydrochloride (636-99-7) + 1-Phenylbut-1-en-3-one (122-57-6) → 4-phenyl-but-3-en-2-one-(4-nitro-phenylhydrazone) (34292-79-0)

Guidance literature:

Reference yield:

→ 4-phenyl-but-3-en-2-one-(4-nitro-phenylhydrazone) (34292-79-0)

Guidance literature:

entspr.Keton,p-Nitrophenylhydrazin;

Reference yield: 50.0%

4-phenyl-but-3-en-2-one-(4-nitro-phenylhydrazone) (34292-79-0) → 1-Phenylbut-1-en-3-one (122-57-6)

Guidance literature:

With Oxone; water; potassium hydrogencarbonate; In acetonitrile; for 1.33333h; Heating;

DOI:10.1080/00304949909355680

upstream raw materials:

4-nitrophenylhydrazine hydrochloride

1-Phenylbut-1-en-3-one

Downstream raw materials:

3-methyl-1-(4-nitro-phenyl)-5-phenyl-4,5-dihydro-1H-pyrazole

3-methyl-1-(4-nitrophenyl)-5-phenyl-1H-pyrazole

1-Phenylbut-1-en-3-one

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