2-Azetidinecarboxylic acid, 1-[(4-methoxyphenyl)methyl]-4-oxo-2-(phenylmethyl)-

Base Information

• Chemical Name: 2-Azetidinecarboxylic acid, 1-[(4-methoxyphenyl)methyl]-4-oxo-2-(phenylmethyl)-
• CAS No.: 344765-39-5
• Molecular Formula: C19H19NO4
• Molecular Weight: 325.364

Synonyms:

Chemical Property of 2-Azetidinecarboxylic acid, 1-[(4-methoxyphenyl)methyl]-4-oxo-2-(phenylmethyl)-

Chemical Property:

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Technology Process of 2-Azetidinecarboxylic acid, 1-[(4-methoxyphenyl)methyl]-4-oxo-2-(phenylmethyl)-

There total 10 articles about 2-Azetidinecarboxylic acid, 1-[(4-methoxyphenyl)methyl]-4-oxo-2-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-benzyl-1-(4-methoxy)benzyl-4-methoxycarbonyl-2-azetidinone (344765-25-9) → 4-benzyl-1-(p-methoxybenzyl)-4-carboxy-2-azetidinone (344765-39-5)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃;

DOI:10.1021/jo015559b

Reference yield: 85.0%

4-benzyl-1-(4-methoxy)benzyl-4-tert-butoxycarbonyl-2-azetidinone (344765-24-8) → 4-benzyl-1-(p-methoxybenzyl)-4-carboxy-2-azetidinone (344765-39-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jo015559b

Reference yield: 61.0%

4-benzyl-1-(4-methoxy)benzyl-4-benzyloxycarbonyl-2-azetidinone (344765-26-0) → 4-benzyl-1-(p-methoxybenzyl)-4-carboxy-2-azetidinone (344765-39-5)

Guidance literature:

With aluminium trichloride; In methoxybenzene; at 65 ℃; for 1h;

upstream raw materials:

4-benzyl-1-(4-methoxy)benzyl-4-methoxycarbonyl-2-azetidinone

4-benzyl-1-(4-methoxy)benzyl-4-tert-butoxycarbonyl-2-azetidinone

4-benzyl-1-(4-methoxy)benzyl-4-benzyloxycarbonyl-2-azetidinone

methyl N-(4-methoxy)benzyl-N-chloroacetyl-L-phenylalaninate

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