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2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime

Base Information Edit
  • Chemical Name:2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime
  • CAS No.:348-73-2
  • Molecular Formula:C9H8F3NO
  • Molecular Weight:203.164
  • Hs Code.:2928000090
  • Mol file:348-73-2.mol
2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime

Synonyms:1,1,1-trifluoro-3-phenylpropan-2-one oxime;1,4-Diacetyl-piperidin-oxim;oxime de la trifluoro-methyl benzyl cetone;1,1,1-Trifluor-3-phenyl-aceton-oxim;1,1,1-trifluoro-3-phenyl-acetone oxime;Oxim des 1,4-Diacetyl-piperidins;

Suppliers and Price of 2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 5 raw suppliers
Chemical Property of 2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime Edit
Chemical Property:
  • Melting Point:38-40 °C 
  • Boiling Point:235.5±40.0 °C(Predicted) 
  • PSA:32.59000 
  • Density:1.23±0.1 g/cm3(Predicted) 
  • LogP:2.62160 
Purity/Quality:

99% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of 2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime

There total 4 articles about 2-Propanone, 1,1,1-trifluoro-3-phenyl-, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 1h; Reflux;
DOI:10.1021/jo501658s
Guidance literature:
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere
1.2: 0.25 h / -78 °C / Inert atmosphere
1.3: -78 - 20 °C / Inert atmosphere
2.1: cesium fluoride / N,N-dimethyl-formamide / 12 h / 60 °C / Inert atmosphere; Molecular sieve
3.1: trifluorormethanesulfonic acid / dichloromethane / 12.17 h / 0 - 20 °C / Inert atmosphere
4.1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 2 h / Inert atmosphere; Reflux
With n-butyllithium; trifluorormethanesulfonic acid; hydroxylamine hydrochloride; sodium acetate; cesium fluoride; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2013.05.078
Guidance literature:
Multi-step reaction with 2 steps
1: trifluorormethanesulfonic acid / dichloromethane / 12.17 h / 0 - 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 2 h / Inert atmosphere; Reflux
With trifluorormethanesulfonic acid; hydroxylamine hydrochloride; sodium acetate; In ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2013.05.078
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