Piperidine, 1-[chloro(triphenylgermyl)boryl]-2,2,6,6-tetramethyl-

Base Information

Chemical Name:Piperidine, 1-[chloro(triphenylgermyl)boryl]-2,2,6,6-tetramethyl-
CAS No.:351345-75-0
Molecular Formula:C₂₇H₃₃BClGeN
Molecular Weight:490.42
Hs Code.:

Synonyms:

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Chemical Property of Piperidine, 1-[chloro(triphenylgermyl)boryl]-2,2,6,6-tetramethyl-

Chemical Property:

Purity/Quality:

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Technology Process of Piperidine, 1-[chloro(triphenylgermyl)boryl]-2,2,6,6-tetramethyl-

There total 2 articles about Piperidine, 1-[chloro(triphenylgermyl)boryl]-2,2,6,6-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 351345-73-8
triphenylgermyllithium-diethylether(1/3)

: 79855-29-1
dichloro-(2,2,6,6,-tetramethylpiperidino)borane

: 351345-75-0
(chloro)-(2,2,6,6,-tetramethylpiperidino)(triphenylgermyl)borane

Guidance literature:: In diethyl ether; hexane; byproducts: LiCl; all manipulations under N2 or Ar; freshly prepd. stirred soln. of Ge compd. in Et2O cooled to -78°C, soln. of borazine derivative in hexane added slowly, mixt. stirred for 1 h at ambient temp.; all volatiles evapd. in vac., residue treated with hexane, filtered, filtrate concd., cooled to -30°C, allowed to stand for several d; elem. anal.;
DOI:10.1002/1521-3749(200105)627:5<1003::AID-ZAAC1003>3.0.CO;2-E

Reference yield:

: 2816-43-5
triphenylgermane

: 351345-75-0
(chloro)-(2,2,6,6,-tetramethylpiperidino)(triphenylgermyl)borane

Guidance literature:: Multi-step reaction with 2 steps

1: hexane; diethyl ether

2: hexane; diethyl ether

In diethyl ether; hexane;
DOI:10.1002/1521-3749(200105)627:5<1003::AID-ZAAC1003>3.0.CO;2-E

Reference yield:

: 351345-73-8
triphenylgermyllithium-diethylether(1/3)

: 351345-75-0
(chloro)-(2,2,6,6,-tetramethylpiperidino)(triphenylgermyl)borane

: 351345-76-1
(2,2,6,6,-tetramethylpiperidino)bis(triphenylgermyl)borane

Guidance literature:: byproducts: LiCl; all manipulations under N2 or Ar; reacted equimolar amts. of starting compds.;
DOI:10.1002/1521-3749(200105)627:5<1003::AID-ZAAC1003>3.0.CO;2-E