cis-2-Aminocyclopentanecarboxylic acid, N-FMOC protected

Base Information

• Chemical Name: cis-2-Aminocyclopentanecarboxylic acid, N-FMOC protected
• CAS No.: 352707-76-7
• Molecular Formula: C₂₁H₂₁NO₄
• Molecular Weight: 351.402
• Hs Code.: 29225090
• Mol file: 352707-76-7.mol

Synonyms:cis-2-Aminocyclopentanecarboxylic acid,N-FMOC protected;CIS-2-(9-FLUORENYLMETHOXYCARBONYLAMINO)CYCLOPENTANECARBOXYLIC ACID;

Chemical Property of cis-2-Aminocyclopentanecarboxylic acid, N-FMOC protected

Chemical Property:

• Vapor Pressure: 1.6E-14mmHg at 25°C
• Boiling Point: 584.8oC at 760 mmHg
• Flash Point: 307.5oC
• PSA: 75.63000
• Density: 1.32g/cm3
• LogP: 4.16930

Purity/Quality:

97% ^*data from raw suppliers

cis-Fmoc-2-amino-1-cyclopentanecarboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of cis-2-Aminocyclopentanecarboxylic acid, N-FMOC protected

There total 29 articles about cis-2-Aminocyclopentanecarboxylic acid, N-FMOC protected which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) + (±)-cis-2-aminocyclopentane-1-carboxylic acid hydrochloride (128052-92-6,158414-44-9,359849-58-4,18414-30-7) → Fmoc-cis-2-amino-1-cyclopentanecarboxylic acid (282524-97-4,352707-76-7)

Guidance literature:

(±)-cis-2-aminocyclopentane-1-carboxylic acid hydrochloride; With potassium hydrogencarbonate; In water; at 20 ℃;

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide; In water; acetonitrile; at 20 ℃;

DOI:10.1021/op010204f

Reference yield: 83.0%

cis-2-aminocyclopentanecarboxylic acid (37910-65-9) → Fmoc-cispentacin (282524-97-4,352707-76-7)

Guidance literature:

With sodium hydrogencarbonate; In water; acetone; at 0 - 20 ℃;

DOI:10.1021/acs.langmuir.8b04250

Reference yield: 70.0%

(1S,2S)-2-hydroxymethyl-cyclopentyl-(9H-fluoren-9-ylmethoxy)-carbamate (359586-63-3) → (1S,2S)-2-(9H-fluoren-9-ylmethoxycarbonyl)amino-cyclopentanecarboxylic acid (359586-64-4,282524-97-4,352707-76-7)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; tetrabutylammomium bromide; In dichloromethane; water; for 1h;

DOI:10.1021/jo010279h

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(±)-cis-2-aminocyclopentane-1-carboxylic acid hydrochloride

cis-2-aza-3-oxobicyclo<3.2.0>heptane

cyclopentene

Downstream raw materials:

(1R,2R)-2-aminocyclopentanecarboxamide

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