Technology Process of Benzene, 1-(chloromethoxy)-4-methoxy-
There total 7 articles about Benzene, 1-(chloromethoxy)-4-methoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus pentachloride; dibenzoyl peroxide;
In
tetrachloromethane;
Heating;
DOI:10.1016/j.bmcl.2005.10.045
- Guidance literature:
-
With
thionyl chloride;
In
dichloromethane;
for 1.5h;
Ambient temperature;
further reagent acetyl chloride;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 52 percent / sodium hydride, sodium iodide / 1,2-dimethoxy-ethane / 6 h / Ambient temperature
2: 89 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.17 h / 0 °C
3: 65 percent / thionyl chloride / CH2Cl2 / 1.5 h / Ambient temperature; further reagent acetyl chloride
With
thionyl chloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; sodium iodide;
In
1,2-dimethoxyethane; dichloromethane;
