2,3-Dinitronaphthalene

Base Information

• Chemical Name: 2,3-Dinitronaphthalene
• CAS No.: 1875-63-4
• Molecular Formula: C10H6N2O4
• Molecular Weight: 218.169
• DSSTox Substance ID: DTXSID30172062
• Nikkaji Number: J119.291D
• Wikidata: Q27122166
• Metabolomics Workbench ID: 57487
• Mol file: 1875-63-4.mol

Synonyms:2,3-Dinitronaphthalene;NAPHTHALENE, 2,3-DINITRO-;1875-63-4;SCHEMBL11203665;CHEBI:50644;DTXSID30172062;Q27122166

Chemical Property of 2,3-Dinitronaphthalene

Chemical Property:

• Vapor Pressure: 4.1E-07mmHg at 25°C
• Boiling Point: 427.4°Cat760mmHg
• Flash Point: 226°C
• PSA: 91.64000
• Density: 1.481g/cm³
• LogP: 3.70260
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 218.03275668
• Heavy Atom Count: 16
• Complexity: 266

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C=C(C(=CC2=C1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 2,3-Dinitronaphthalene

There total 2 articles about 2,3-Dinitronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

naphthalene (91-20-3,71998-51-1,72931-45-4) → 1-Nitronaphthalene (86-57-7) + 2,4-dinitronaphthalene (606-37-1) + 2-nitronaphthalene (581-89-5) + 2,3-dinitronaphthalene (1875-63-4)

Guidance literature:

With 2,6-di-tert-butyl-pyridine; Nitrogen dioxide; In tetrachloromethane; at 25 ℃; for 24h; Product distribution; Mechanism; var. 1- and 2-nitronaphthalenes; other solvents, temperatures and times;

DOI:10.1021/jo00264a009

Reference yield:

naphthalene (91-20-3,71998-51-1,72931-45-4) → 1-Nitronaphthalene (86-57-7) + 1,8-dinitronaphthalene (602-38-0) + 2,4-dinitronaphthalene (606-37-1) + 2,3-dinitronaphthalene (1875-63-4)

Guidance literature:

With sodium nitrate; silver nitrate; potassium nitrate; potassium hexacyanoferrate(III); at 160 ℃; for 1h; Further byproducts.;

DOI:10.1021/jo800839f

Reference yield:

2,3-dinitronaphthalene (1875-63-4) → 3-nitronaphthalen-2-amine (13115-28-1)

Guidance literature:

With methanol; sodium disulfide;

upstream raw materials:

naphthalene

Downstream raw materials:

3-nitronaphthalen-2-amine

2-Chlor-3-nitro-naphthalin

3-chloronaphthalene-2-amine