Duguenaine

Base Information

• Chemical Name: Duguenaine
• CAS No.: 80550-24-9
• Molecular Formula: C19H15NO3
• Molecular Weight: 305.33
• Mol file: 80550-24-9.mol

Synonyms:

Chemical Property of Duguenaine

Chemical Property:

• PSA: 30.93000
• LogP: 3.63690

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Duguenaine

There total 2 articles about Duguenaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1,2-methylenedioxy-6a,7-dehydronoraporphine (41679-82-7) → duguenaine (80550-24-9)

Guidance literature:

With formaldehyd; In water; for 24h; Ambient temperature;

Reference yield:

ethyl 6,7-dihydro-5H-benzo-1,3-benzodioxolo<6,5,4-de>quinoline-7-carboxylate (87201-29-4) → duguenaine (80550-24-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / KOH, EtOH / 18 h / Heating

2: 76 percent / 37percent formaldehyde / H₂O / 24 h / Ambient temperature

With potassium hydroxide; formaldehyd; ethanol; In water;

upstream raw materials:

1,2-methylenedioxy-6a,7-dehydronoraporphine

ethyl 6,7-dihydro-5H-benzo-1,3-benzodioxolo<6,5,4-de>quinoline-7-carboxylate

Refernces