4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole

Base Information

Chemical Name:4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole
CAS No.:73424-89-2
Molecular Formula:C₁₃H₁₆N₂O₂S
Molecular Weight:264.348
Hs Code.:
DSSTox Substance ID:DTXSID00994152

Synonyms:BRN 0549863;4-((Methylamino)methyl)-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole 1,1-dioxide;4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole;N-Methyl-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole-4-methylamine 1,1-dioxide;Thiopyrano(2,3-b)indole, 2,3,4,9-tetrahydro-4-((methylamino)methyl)-, 1,1-dioxide;Thiopyrano(2,3-b)indole-4-methylamine, 2,3,4,9-tetrahydro-N-methyl-, 1,1-dioxide;73424-89-2;DTXSID00994152;LS-153298;4-[(Methylamino)methyl]-2,3,4,9-tetrahydro-1H-1lambda~6~-thiopyrano[2,3-b]indole-1,1-dione

Suppliers and Price of 4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole

Chemical Property:

Vapor Pressure:1.48E-10mmHg at 25°C
Boiling Point:511°Cat760mmHg
Flash Point:262.8°C
Density:1.31g/cm³
XLogP3:1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:264.09324893
Heavy Atom Count:18
Complexity:404

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CNCC1CCS(=O)(=O)C2=C1C3=CC=CC=C3N2

Technology Process of 4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole

There total 4 articles about 4-(N-Methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano(2,3-b)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73425-25-9
4-(N-tert-butoxycarbonyl-N-methylaminomethyl)-2,3,4,9-tetrahydrothiopyrano<2,3-b>indole

: 73424-89-2
4-(N-methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano<2,3-b>indole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; Yield given. Multistep reaction; 1.) m-chloroperbenzoic acid, CHCl₃, RT, 3h; 2.) CH₂Cl, CF₃COOH, RT, 2h;
DOI:10.1248/cpb.32.877

Reference yield:

: 73425-49-7
4-aminomethyl-2,3,4,9-tetrahydrothiopyrano<2,3-b>indole

: 73424-89-2
4-(N-methylaminomethyl)-1,1-dioxo-2,3,4,9-tetrahydrothiopyrano<2,3-b>indole

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / tetrahydrofuran / 1 h / Ambient temperature

2: 1.) m-chloroperbenzoic acid; 2.) CF₃COOH / 1.) m-chloroperbenzoic acid, CHCl₃, RT, 3h; 2.) CH₂Cl, CF₃COOH, RT, 2h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1248/cpb.32.877