6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran

Base Information

Chemical Name:6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran
CAS No.:83359-44-8
Molecular Formula:C₁₅H₁₁NO₂
Molecular Weight:237.258
Hs Code.:2926909090
DSSTox Substance ID:DTXSID401003358
Mol file:83359-44-8.mol

Synonyms:83359-44-8;FCE 20518;6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran;6-(Hydroxymethyl)-6H-dibenzo(b,d)pyran-6-carbonitrile;6H-Dibenzo(b,d)pyran-6-carbonitrile, 6-(hydroxymethyl)-;6-(HYDROXYMETHYL)-6H-DIBENZO[B,D]PYRAN-6-CARBONITRILE;SCHEMBL11102258;DTXSID401003358;LS-61143

Suppliers and Price of 6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
6-(HYDROXYMETHYL)-6H-DIBENZO(B,D)PYRAN-6-CARBONITRILE 95.00%
5MG
$ 500.32

Total 4 raw suppliers

Chemical Property of 6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran

Chemical Property:

Vapor Pressure:2.73E-10mmHg at 25°C
Boiling Point:486.8°Cat760mmHg
Flash Point:248.2°C
PSA：53.25000
Density:1.33g/cm³
LogP:2.45718
XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:237.078978594
Heavy Atom Count:18
Complexity:361

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

6-(HYDROXYMETHYL)-6H-DIBENZO(B,D)PYRAN-6-CARBONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=CC=CC=C3OC2(CO)C#N

Technology Process of 6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran

There total 4 articles about 6-Cyano-6-hydroxymethyl-6H-dibenzo(b,d)pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 83358-33-2
6H-dibenzopyran-6-carbonitrile

: 83359-44-8
6H-6-hydroxymethyl-dibenzopyran-6-carbonitrile

Guidance literature:: With sodium methylate; In dimethyl sulfoxide; at 20 - 25 ℃; for 5h;

Reference yield:

: 83358-33-2
6H-dibenzopyran-6-carbonitrile

: 83359-44-8
6H-6-hydroxymethyl-dibenzopyran-6-carbonitrile

Guidance literature:: With sodium methylate; paraformaldehyde; In dimethyl sulfoxide;

Reference yield:

: 2005-10-9
6H-benzo[c]chromen-6-one

: 83359-44-8
6H-6-hydroxymethyl-dibenzopyran-6-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 1.2M diisobutyl aluminium hydride / toluene / 1 h / -70 °C

2: 90 percent / ZnI₂ / benzene / 0.5 h / Ambient temperature

3: 91 percent / sodium methylate / dimethylsulfoxide / 5 h / 20 - 25 °C

With sodium methylate; diisobutylaluminium hydride; zinc(II) iodide; In dimethyl sulfoxide; toluene; benzene;