8-Fluoranthenecarboxylic acid, 9-amino-7,10-bis(4-dodecylphenyl)-

Base Information

Chemical Name:8-Fluoranthenecarboxylic acid, 9-amino-7,10-bis(4-dodecylphenyl)-
CAS No.:373360-41-9
Molecular Formula:C53H67NO2
Molecular Weight:750.12
Hs Code.:

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Chemical Property of 8-Fluoranthenecarboxylic acid, 9-amino-7,10-bis(4-dodecylphenyl)-

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Technology Process of 8-Fluoranthenecarboxylic acid, 9-amino-7,10-bis(4-dodecylphenyl)-

There total 2 articles about 8-Fluoranthenecarboxylic acid, 9-amino-7,10-bis(4-dodecylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7,11-bis-(4-dodecyl-phenyl)-9-aza-cyclopenta[k]fluoranthene-8,10-dione

: 373360-41-9
8-amino-7,10-di-p-dodecylphenylfluoranthene-9-carboxylic acid

Guidance literature:: 7,11-bis-(4-dodecyl-phenyl)-9-aza-cyclopenta[k]fluoranthene-8,10-dione; With sodium hydroxide; sodium hypochlorite; In methanol; water; for 0.166667h; Heating;

With potassium hydroxide; In propan-1-ol; for 72h; Further stages.; Heating;
DOI:10.1021/ol016391j

Reference yield:

: 189139-45-5
7,9-Bis(4-dodecylphenyl)-8H-cyclopenta[l]acenaphthylen-8-one

: 373360-41-9
8-amino-7,10-di-p-dodecylphenylfluoranthene-9-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromobenzene / Heating

1.2: 78 percent / Br₂ / 3 h / Heating

2.1: NaOH; NaOCl / methanol; H₂O / 0.17 h / Heating

2.2: 62 percent / KOH / propan-1-ol / 72 h / Heating

With sodium hydroxide; sodium hypochlorite; bromobenzene; In methanol; water; 1.1: Diels-Alder reaction / 2.2: Hoffmann rearrangement;
DOI:10.1021/ol016391j