3-Acetylpyrrhoxanthinol

Base Information

Chemical Name:3-Acetylpyrrhoxanthinol
CAS No.:54369-13-0
Molecular Formula:C₃₉H₄₈O₆
Molecular Weight:612.807
Hs Code.:
Mol file:54369-13-0.mol

Synonyms:

Suppliers and Price of 3-Acetylpyrrhoxanthinol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 3-Acetylpyrrhoxanthinol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Acetylpyrrhoxanthinol

There total 24 articles about 3-Acetylpyrrhoxanthinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20548-02-1
trans (4R,6R)-4-hydroxy-2,2,6-trimethylcyclohexanone

: 54369-13-0,128386-33-4,128386-34-5,128386-35-6,128386-44-7,142759-42-0
Acetic acid 4-{(3E,5E,7E,9E)-11-[4-[(E)-2-((1S,4S,6R)-4-hydroxy-2,2,6-trimethyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-vinyl]-5-oxo-5H-furan-(2Z)-ylidene]-3,10-dimethyl-undeca-3,5,7,9-tetraen-1-ynyl}-3,5,5-trimethyl-cyclohex-3-enyl ester

Guidance literature:: Multi-step reaction with 12 steps

1: 93 percent / Et₃N, dimethylaminopyridine / CH₂Cl₂

2: 89 percent / LDA / tetrahydrofuran

3: 93 percent / Et₃N / PdCl₂(PPh₃)2 / dimethylformamide

4: LiAlH₄ / diethyl ether

5: pyridine

6: 89 percent / Pd(PPh₃)4 / tetrahydrofuran; methanol

7: 1) BuLi, 2) NaH / 1) THF, 2) DMF

8: 84 percent / Bu₄NF / tetrahydrofuran

9: 1) OsO₄-NaIO₄, 2) Al₂O₃ / 1) dioxane-H₂O

10: 79 percent / I₂ / diethyl ether; hexane

11: 19 percent / m-chloroperbenzoic acid / CH₂Cl₂

12: 1) LDA / 1) THF, hexane, 2) -78 deg C

With pyridine; dmap; aluminum oxide; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; iodine; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 20548-02-1
trans (4R,6R)-4-hydroxy-2,2,6-trimethylcyclohexanone

: 54369-13-0,128386-33-4,128386-34-5,128386-35-6,128386-44-7,142759-42-0
pyrrhoxanthin

Guidance literature:: Multi-step reaction with 12 steps

1: 93 percent / Et₃N, dimethylaminopyridine / CH₂Cl₂

2: 89 percent / LDA / tetrahydrofuran

3: 93 percent / Et₃N / PdCl₂(PPh₃)2 / dimethylformamide

4: LiAlH₄ / diethyl ether

5: pyridine

6: 89 percent / Pd(PPh₃)4 / tetrahydrofuran; methanol

7: 1) BuLi, 2) NaH / 1) THF, 2) DMF

8: 84 percent / Bu₄NF / tetrahydrofuran

9: 1) OsO₄-NaIO₄, 2) Al₂O₃ / 1) dioxane-H₂O

10: 79 percent / I₂ / diethyl ether; hexane

11: 19 percent / m-chloroperbenzoic acid / CH₂Cl₂

12: 1) LDA / 1) THF, hexane, 2) -78 deg C

With pyridine; dmap; aluminum oxide; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; iodine; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 146566-70-3
4-tert-Butyldimethylsilyloxy-2,2,6-trimethylcyclohexanone

: 54369-13-0,128386-33-4,128386-34-5,128386-35-6,128386-44-7,142759-42-0
Acetic acid 4-{(3E,5E,7E,9E)-11-[4-[(E)-2-((1S,4S,6R)-4-hydroxy-2,2,6-trimethyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-vinyl]-5-oxo-5H-furan-(2Z)-ylidene]-3,10-dimethyl-undeca-3,5,7,9-tetraen-1-ynyl}-3,5,5-trimethyl-cyclohex-3-enyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 89 percent / LDA / tetrahydrofuran

2: 93 percent / Et₃N / PdCl₂(PPh₃)2 / dimethylformamide

3: LiAlH₄ / diethyl ether

4: pyridine

5: 89 percent / Pd(PPh₃)4 / tetrahydrofuran; methanol

6: 1) BuLi, 2) NaH / 1) THF, 2) DMF

7: 84 percent / Bu₄NF / tetrahydrofuran

8: 1) OsO₄-NaIO₄, 2) Al₂O₃ / 1) dioxane-H₂O

9: 79 percent / I₂ / diethyl ether; hexane

10: 19 percent / m-chloroperbenzoic acid / CH₂Cl₂

11: 1) LDA / 1) THF, hexane, 2) -78 deg C

With pyridine; aluminum oxide; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; iodine; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;