4-Piperidinebutanoic acid, 1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester

Base Information

Chemical Name:4-Piperidinebutanoic acid, 1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester
CAS No.:374776-41-7
Molecular Formula:C28H41N5O7S
Molecular Weight:591.729
Hs Code.:

4-Piperidinebutanoic acid,
1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb
onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester

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Chemical Property of 4-Piperidinebutanoic acid, 1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester

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Technology Process of 4-Piperidinebutanoic acid, 1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester

There total 2 articles about 4-Piperidinebutanoic acid, 1-[[3-[[[5-(aminocarbonyl)-1-methyl-3-propyl-1H-pyrazol-4-yl]amino]carb onyl]-4-ethoxyphenyl]sulfonyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 91370-63-7
ethyl 4-(piperidin-4-yl)butyrate

: 226956-42-9
4-(5-chlorosulfonyl-2-ethoxybenzamido)-1-methyl-3-n-propylpyrazole-5-carboxamide

: 374776-41-7
4-(2-ethoxy-5-(4-(3-ethoxycarbonylpropyl)piperidinylsulfonyl)benzamido)-1-methyl-3-n-propylpyrazole-5-carboxamide

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(01)00200-0

Reference yield:

: 139756-03-9
4-[(2-ethoxybenzoyl)amino]-1-methyl-3-propyl-1H-pyrazole-5-carboxamide

: 374776-41-7
4-(2-ethoxy-5-(4-(3-ethoxycarbonylpropyl)piperidinylsulfonyl)benzamido)-1-methyl-3-n-propylpyrazole-5-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ClSO₃H / 2 h / 0 - 2 °C

2: 76 percent / Et₃N / ethanol / 2 h / 20 °C

With chlorosulfonic acid; triethylamine; In ethanol;
DOI:10.1016/S0968-0896(01)00200-0