Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl-

Base Information

• Chemical Name: Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl-
• CAS No.: 375395-22-5
• Molecular Formula: C13H19N
• Molecular Weight: 189.301
• DSSTox Substance ID: DTXSID90477484
• Nikkaji Number: J1.935.239K

Synonyms:375395-22-5;Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl-;DTXSID90477484;LRJFENJNBIDXQZ-UHFFFAOYSA-N;2-n-Propyl-1,2,3,4-tetrahydro-1-methylquinoline

Chemical Property of Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl-

Chemical Property:

• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 189.151749610
• Heavy Atom Count: 14
• Complexity: 178

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC1CCC2=CC=CC=C2N1C

Technology Process of Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl-

There total 1 articles about Quinoline, 1,2,3,4-tetrahydro-1-methyl-2-propyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ethylmagnesium bromide (925-90-6) + 2-bromomethyl-1-methyl-1,2,3,4-tetrahydroquinoline (618113-50-1) → 1-methyl-2-propyl-1,2,3,4-tetrahydroquinoline (375395-22-5) + N-(2-but-3-enylphenyl)-N-methylamine + 1,2-Dimethyl-1,2,3,4-tetrahydroquinoline (16055-19-9)

Guidance literature:

With lithium chloride; copper dichloride; In tetrahydrofuran; at -5 - 20 ℃; for 5h;

DOI:10.1016/S0040-4020(03)00915-3

Reference yield:

1-methyl-2-propyl-1,2,3,4-tetrahydroquinoline (375395-22-5) → 2-n-Propyl-1,2,3,4-tetrahydroquinoline (76916-51-3)

Guidance literature:

Multi-step reaction with 2 steps

2: concentrated hydrochloric acid / 110 °C

With hydrogenchloride;

upstream raw materials:

ethylmagnesium bromide

2-bromomethyl-1-methyl-1,2,3,4-tetrahydroquinoline

Downstream raw materials:

2-n-Propyl-1,2,3,4-tetrahydroquinoline

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