1,1,3,3-Tetranitropropane

Base Information

• Chemical Name: 1,1,3,3-Tetranitropropane
• CAS No.: 3759-59-9
• Molecular Formula: C3H4N4O8
• Molecular Weight: 224.087
• Mol file: 3759-59-9.mol

Synonyms:1,1,3,3-tetra-n-butyl-1,3-di(n-butyloxy)distannoxane;1,1,3,3-tetranitro-propane;1,1,3,3-Tetranitropropan;1,1,3,3-tetra-n-butyl-1,3-bi(n-butyloxy) distannoxane;1,1,3,3-tetrabutyl-1,3-di(butyloxy)-distannoxane;1,1,3,3-Tertranitro-propan;1,1,3,3-tetrabutyl-1,3-dibutoxy-distannoxane;Distannoxane,1,3-dibutoxy-1,1,3,3-tetrabutyl;

Chemical Property of 1,1,3,3-Tetranitropropane

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 340.679oC at 760 mmHg
• Flash Point: 175.67oC
• PSA: 183.28000
• Density: 1.725g/cm3
• LogP: 1.22830

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,3,3-Tetranitropropane

There total 5 articles about 1,1,3,3-Tetranitropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dibromo-1,1,3,3-tetranitro-propane (1067-04-5) → 1,1,3,3-tetranitropropane (3759-59-9)

Guidance literature:

With potassium cyanide; In methanol; water;

DOI:10.1021/jo01069a045

Reference yield:

1,1,3,3-tetranitropropane dipotassium salt (6928-37-6) → 1,1,3,3-tetranitropropane (3759-59-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; Yield given; 1) -60 to -50 deg C, 1h, 2) -50 to -30 deg C, 1h, 3) -30 deg C to RT, 1-2h;

Reference yield:

2,2-dinitro-ethylamine (10119-99-0) → 1,1,3,3-tetranitropropane (3759-59-9)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/jo01066a619

upstream raw materials:

1,3-dibromo-1,1,3,3-tetranitro-propane

2,2-dinitro-ethylamine

potassium 1,1,3,3-tetranitropropane-1,3-diide

1,1,3,3-tetranitropropane dipotassium salt

Refernces

• 1、 Kamlet,M.J.,Dacons,J.C.. "-". . p. 3005 - 3008. Retrieved 1961.