N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine

Base Information

Chemical Name:N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine
CAS No.:37627-92-2
Molecular Formula:C8H8ClN5
Molecular Weight:209.638
Hs Code.:
European Community (EC) Number:829-462-9
DSSTox Substance ID:DTXSID001323924
Nikkaji Number:J2.013.767C
ChEMBL ID:CHEMBL14435
Mol file:37627-92-2.mol

Synonyms:37627-92-2;N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine;3-N-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine;GNF-PF-3836;N3-(3-chlorophenyl)-4H-1,2,4-triazole-3,5-diamine;N-(5-amino-1H-1,2,4-triazol-3-yl)-N-(3-chlorophenyl)amine;MLS000861590;CHEMBL14435;SCHEMBL6743326;SCHEMBL14869336;N~3~-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine;RPFUCBPCSIJVSM-UHFFFAOYSA-N;DTXSID001323924;HMS2777A17;MFCD00104000;STL436145;AKOS015867417;LS-09465;SMR000460374;FT-0756422;EN300-219607;N-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine;N-(3-chlorophenyl)-4H-1,2,4-triazole-3,5-diamine;Z2182115386;N*3*-(3-Chloro-phenyl)-1H-[1,2,4]triazole-3,5-diamine;N-(5-amino-4H-1,2,4-triazol-3-yl)-N-(3-chlorophenyl)amine

Suppliers and Price of N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:209.0468230
Heavy Atom Count:14
Complexity:191

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)NC2=NNC(=N2)N

Technology Process of N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine

There total 3 articles about N3-(3-chlorophenyl)-1H-1,2,4-triazole-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72500-48-2
methyl N-(3-chlorophenyl)-N′-cyanocarbamimidothioate

: 37627-92-2
N³-(3-chlorophenyl)-1H-[1,2,4]triazole-3,5-diamine

Guidance literature:: With hydrazine hydrate; In isopropyl alcohol; for 1h; Reflux;
DOI:10.1134/S1070427220080078

Reference yield:

: 2392-68-9
3-chlorophenyl-isothiocyanate

: 37627-92-2
N³-(3-chlorophenyl)-1H-[1,2,4]triazole-3,5-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.25 h / 20 °C / 760.05 Torr / Inert atmosphere

1.2: 0.42 h / 20 °C / 760.05 Torr / Inert atmosphere

1.3: 3.33 h / 20 °C / 760.05 Torr / Inert atmosphere

2.1: hydrazine / ethanol / 1 h / 65 °C / 760.05 Torr / Inert atmosphere

With sodium methylate; hydrazine; In methanol; ethanol;