Cyclohexanamine, 3,3-dimethyl-

Base Information

• Chemical Name: Cyclohexanamine, 3,3-dimethyl-
• CAS No.: 37694-43-2
• Molecular Formula: C8H17N
• Molecular Weight: 127.23
• Mol file: 37694-43-2.mol

Synonyms:

Chemical Property of Cyclohexanamine, 3,3-dimethyl-

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanamine, 3,3-dimethyl-

There total 5 articles about Cyclohexanamine, 3,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethylcyclohexanone oxime (4994-14-3) → 3,3-dimethylcyclohexan-1-amine (37694-43-2)

Guidance literature:

With hydrogen; nickel;

Reference yield:

3,3-dimethylcyclohexanone (2979-19-3) → 3,3-dimethylcyclohexan-1-amine (37694-43-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride, sodium acetate / methanol; H₂O / 1 h / Heating

2: lithium aluminium hydride / diethyl ether / 24 h / Heating

With lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; In methanol; diethyl ether; water;

Reference yield:

3,3-dimethylcyclohexanol (767-12-4) → 3,3-dimethylcyclohexan-1-amine (37694-43-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / Jones reagent / acetone / 1.) 0 deg.C, 2 h.; 2.) 2 h. room temp

2: hydroxylamine hydrochloride, sodium acetate / methanol; H₂O / 1 h / Heating

3: lithium aluminium hydride / diethyl ether / 24 h / Heating

With lithium aluminium tetrahydride; jones reagent; hydroxylamine hydrochloride; sodium acetate; In methanol; diethyl ether; water; acetone;

upstream raw materials:

3,3-dimethylcyclohexanone oxime

3,3-dimethylcyclohexanone

3,3-dimethylcyclohexanol

dimedone

Downstream raw materials:

3,3-Dimethyl-N,N-dimethylcyclohexylamin

3,3-dimethylcyclohexylthiourea

ethyl 1-(3,3-dimethylcyclohexyl)-1H-imidazole-4-carboxylate