2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride

Base Information

Chemical Name:2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride
CAS No.:39157-07-8
Molecular Formula:C10H8ClNO3
Molecular Weight:225.631
Hs Code.:
DSSTox Substance ID:DTXSID70706183

Synonyms:2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride;39157-07-8;DTXSID70706183

Suppliers and Price of 2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:225.0192708
Heavy Atom Count:15
Complexity:288

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC1=CC=C(C=C1)[N+](=O)[O-])C(=O)Cl

Technology Process of 2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride

There total 7 articles about 2-Methyl-3-(4-nitrophenyl)prop-2-enoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949-98-4
2-methyl-3-(4-nitrophenyl)acrylic acid

: 39157-07-8
(Z)-2-Methyl-3-(4-nitro-phenyl)-acryloyl chloride

Guidance literature:: With thionyl chloride; at 0 ℃; for 2h; Reflux;
DOI:10.1016/j.ejmech.2014.03.020

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 39157-07-8
(Z)-2-Methyl-3-(4-nitro-phenyl)-acryloyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / pyridine / 4 h / 90 °C

2: thionyl chloride / 2 h / 0 °C / Reflux

With piperidine; thionyl chloride; In pyridine;
DOI:10.1016/j.ejmech.2014.03.020